n-butyllithium 1.) THF, hexane, from -78 deg C to RT, 1 h, 2.) THF, hexane, RT, 2 h; Yield given. Multistep reaction. Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 116, # 22 p. 9869 - 9882
[Rh(2,5-norbornadiene)(chloride)(1-(2-NHBoc-ethyl)-3-benzyl-imidazolin-2-ylidene)] in chloroform-d1 T=25°C; 2 h; Inert atmosphere; optical yield given as percent de;