2-氯-4,6-二甲基-5-硝基烟腈合成路线 （共 5 条）
反应条件
trichlorophosphate
T=180°C;
参考文献
Dyadyuchenko; Strelkov; Mikhailichenko; Zaplishny
Chemistry of Heterocyclic Compounds, 2004 , vol. 40, # 3 p. 308 - 314
反应条件
1: 54 percent / HNO3 / acetic anhydride / 1 h / 5 - 20 °C
2: 61 percent / POCl3 / 180 °C
View Scheme
参考文献
Dyadyuchenko; Strelkov; Mikhailichenko; Zaplishny
Chemistry of Heterocyclic Compounds, 2004 , vol. 40, # 3 p. 308 - 314
反应条件
1: ethanol; piperidine
2: acetic acid anhydride; fuming HNO3
3: chlorobenzene; PCl5
View Scheme
参考文献
van Wagtendonk; Wibaut
Recueil des Travaux Chimiques des Pays-Bas, 1942 , vol. 61, p. 728,731
反应条件
palladium on activated charcoal; ethanol; platinum
Hydrogenation;
参考文献
van Wagtendonk; Wibaut
Recueil des Travaux Chimiques des Pays-Bas, 1942 , vol. 61, p. 728,731
反应条件
ethanol; sulfuric acid; zinc
参考文献
Merck,E.
Patent: DE707266 , 1939 ;
DRP/DRBP Org.Chem.
