(S)-3-丁烯-1,2-二醇合成路线 （共 20 条）
反应条件
Dowex 50X8-200 acidic ion-exchange resin in methanol 23 h; Ambient temperature;
参考文献
Bergmeier, Stephen C.; Stanchina, Dionne M.
Journal of Organic Chemistry, 1999 , vol. 64, # 8 p. 2852 - 2859
反应条件
Pseudomonas putida ML 2; wild type strain in phosphate buffer T=4°C; Addition; dihydroxylation; pH=7.5; 24 h; Enzymatic reaction; Title compound not separated from byproducts;
参考文献
Boyd, Derek R.; Clarke, David; Cleij, Marcel C.; Hamilton, John T.G.; Sheldrake, Gary N.
Monatshefte fur Chemie, 2000 , vol. 131, # 6 p. 673 - 685
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran desilylation;
参考文献
Tetrahedron Asymmetry, , vol. 11, # 13 p. 2741 - 2751
反应条件
sodium hydroxide; sodium azide; acid phosphatase; pyruvate kinase; Phosphoenolpyruvate; glycerol kinase from Streptomyces canus; potassium chloride; adenosine 5'-triphosphoric acid; 2-hydroxyethanethiol; magnesium chloride 1.) H2O, 35 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 63, # 12 p. 4039 - 4045
反应条件
sulfuric acid T=5°C; 0.75 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron Asymmetry, , vol. 6, # 1 p. 15 - 16
反应条件
horse liver alcohol dehydrogenase in water T=37°C; Oxidation; pH=7.4; 0.05 h; Enzymatic reaction; Enzyme kineticsProduct distribution;
参考文献
Kemper, Raymond A.; Elfarra, Adnan A.
Chemical Research in Toxicology, 1996 , vol. 9, # 7 p. 1127 - 1134
反应条件
in palladium monocarbide; ethanol
反应条件
in palladium monocarbide; ethanol
参考文献
Schering Corporation
Patent: US5698557 A1, 1997 ;
反应条件
di(n-butyl)tin oxide; triethylamine in dichloromethane T=0°C; 6 h;
参考文献
Jhillu Singh, Yadav; Rao Yarrapothu, Gangadhara; Vemula, Rajender
RSC Advances, 2013 , vol. 3, # 1 p. 55 - 58
反应条件
horse liver alcohol dehydrogenase in water
T=37°C; Oxidation; pH=7.4; 0.05 h; Enzymatic reaction; Enzyme kineticsProduct distribution;
参考文献
Kemper, Raymond A.; Elfarra, Adnan A.
Chemical Research in Toxicology, 1996 , vol. 9, # 7 p. 1127 - 1134
