3,5-二溴噻吩-2-羧酸乙酯合成路线 (共 3 条)
反应条件
sulfuric acid
6 h; Heating;
参考文献
Pereira, Raquel; Furst, Audrey; Iglesias, Beatriz; Germain, Pierre; Gronemeyer, Hinrich; De Lera, Angel R.
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 24 p. 4514 - 4525
反应条件
lithium diisopropyl amide
1.) THF, - 78 deg C, 0.5 h, 2.) THF, - 78 deg C; Yield given. Multistep reaction;
参考文献
Kano, Shinzo; Yuasa, Yoko; Yokomatsu, Tsutomu; Shibuya, Shiroshi
Heterocycles, 1983 , vol. 20, # 10 p. 2035 - 2037
反应条件
lithium aluminium tetrahydride in diethyl ether
T=0°C; 2.5 h;
参考文献
Pereira, Raquel; Furst, Audrey; Iglesias, Beatriz; Germain, Pierre; Gronemeyer, Hinrich; De Lera, Angel R.
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 24 p. 4514 - 4525