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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
62224-82-2
合成路线
(共 7 条)
622-42-4
硝基甲苯
→
反应条件
62224-82-2
反应条件
1: sodium methylate 2: chloroform; acetone; bromine 3: aqueous-methanolic KOH-solution; diethyl ether 4: methanolic KOH-solution; hydroxylamine hydrochloride View Scheme
参考文献
Kohler
Journal of the American Chemical Society, 1924 , vol. 46, p. 1740
Journal of the American Chemical Society, 1925 , vol. 47, p. 3030
96260-76-3
→
反应条件
62224-82-2
反应条件
1: chloroform; acetone; bromine 2: aqueous-methanolic KOH-solution; diethyl ether 3: methanolic KOH-solution; hydroxylamine hydrochloride View Scheme
参考文献
Kohler
Journal of the American Chemical Society, 1924 , vol. 46, p. 1740
Journal of the American Chemical Society, 1925 , vol. 47, p. 3030
861777-28-8
→
反应条件
62224-82-2
反应条件
1: aqueous-methanolic KOH-solution; diethyl ether 2: methanolic KOH-solution; hydroxylamine hydrochloride View Scheme
参考文献
Kohler
Journal of the American Chemical Society, 1924 , vol. 46, p. 1740
Journal of the American Chemical Society, 1925 , vol. 47, p. 3030
94-41-7
苯亚甲基苯乙酮
→
反应条件
62224-82-2
反应条件
1: sodium methylate 2: chloroform; acetone; bromine 3: aqueous-methanolic KOH-solution; diethyl ether 4: methanolic KOH-solution; hydroxylamine hydrochloride View Scheme
参考文献
Kohler
Journal of the American Chemical Society, 1924 , vol. 46, p. 1740
Journal of the American Chemical Society, 1925 , vol. 47, p. 3030
408532-96-7
→
反应条件
62224-82-2
反应条件
1: NaOH-solution; diethyl ether 2: methanolic KOH-solution; hydroxylamine hydrochloride View Scheme
参考文献
Kohler
Journal of the American Chemical Society, 1924 , vol. 46, p. 1740
Journal of the American Chemical Society, 1925 , vol. 47, p. 3030
1167-72-2
→
反应条件
62224-82-2
反应条件
potassium hydroxide; hydroxylamine hydrochloride
参考文献
Kohler
Journal of the American Chemical Society, 1924 , vol. 46, p. 1740
Journal of the American Chemical Society, 1925 , vol. 47, p. 3030
62224-74-2
→
反应条件
62224-82-2
反应条件
hydroxylamine hydrochloride in ethanol
参考文献
Jones,R.A.Y.; Sadighi,N.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1976 , p. 2259 - 2264