2,5-二氯-2,5-二甲基己烷合成路线 （共 77 条）
反应条件
1: 60 percent Turnov. / AlCl3 / 1.67 h / 0 °C
2: 79 percent / Aliquat 336, 40percent aq. NaOH / 22 h / 80 °C
3: 68 percent / 90percent aq. formic acid / 6 h / Heating
View Scheme
参考文献
Mayr, Herbert; Heilmann, Werner; Baeuml, Engelbert; Vorbrueggen, Helmut
Chemische Berichte, 1991 , vol. 124, # 1 p. 203 - 206
反应条件
AlCl3, aluminium chloride in 1,2-dichloro-ethane
T=60°C; 8 h;
参考文献
Chebny, Vincent J.; Navale, Tushar S.; Shukla, Ruchi; Lindeman, Sergey V.; Rathore, Rajendra
Organic Letters, 2009 , vol. 11, # 11 p. 2253 - 2256
参考文献
Weng, Wei; Zhang, Zhencheng; Amine, Khalil
Patent: US2013/288137 A1, 2013 ;
Location in patent: Page/Page column ;
反应条件
1: FeCl3
2: aqueous HCl; concentrated H2SO4
View Scheme
参考文献
Givaudan Corp.
Patent: US2800511 , 1955 ;
反应条件
1: FeCl3
2: aqueous HCl; concentrated H2SO4
3: aqueous hexamethylenetetramine
View Scheme
参考文献
Wood,T.F. et al.
Journal of Organic Chemistry, 1963 , vol. 28, p. 2248 - 2255
反应条件
aluminium trichloride
参考文献
Wood,T.F. et al.
Journal of Organic Chemistry, 1963 , vol. 28, p. 2248 - 2255
参考文献
Henry
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1906 , vol. 143, p. 496
