反应条件
1: 99 percent / 2,6-lutidine / CH2Cl2 / 0 - 20 °C 2: 78 percent / second generation Grubbs' catalyst / CH2Cl2 / 12 h / 40 °C 3: 95 percent / H2 / RhCl(PPh3)3 / benzene / 4 h / 20 °C 4: 90 percent / Et3SiH; BiBr3 / acetonitrile / 1 h / 20 °C 5: 41.0 mg / TBAF / acetonitrile; tetrahydrofuran / 0.17 h View Scheme
参考文献
Evans, P. Andrew; Cui, Jian; Gharpure, Santosh J.
Organic Letters, 2003 , vol. 5, # 21 p. 3883 - 3885
