6-乙酰基-3,4-二氢-2(1h)-喹啉酮合成路线 （共 3 条）
反应条件
potassium carbonate; [pentamethylcyclopentadienylRhCl2]2 in acetone
T=100°C; 20 h;
参考文献
Fujita, Ken-Ichi; Takahashi, Yoshinori; Owaki, Maki; Yamamoto, Kazunari; Yamaguchi, Ryohei
Organic Letters, 2004 , vol. 6, # 16 p. 2785 - 2788
反应条件
aluminium trichloride in carbon disulfide
18 h; Heating;
参考文献
Martinez; Walker; Hirschfeld; Bruno; Yang; Maloney
Journal of Medicinal Chemistry, 1992 , vol. 35, # 4 p. 620 - 628
反应条件
1: 66 percent / Et3N; CuI / PdCl2(PPh3)2 / 4.5 h / 20 °C
2: 48 percent / H2 / Pd/C / methanol / 50 h / 20 °C
3: 96 percent / K2CO3 / [pentamethylcyclopentadienylRhCl2]2 / acetone / 20 h / 100 °C
View Scheme
参考文献
Fujita, Ken-Ichi; Takahashi, Yoshinori; Owaki, Maki; Yamamoto, Kazunari; Yamaguchi, Ryohei
Organic Letters, 2004 , vol. 6, # 16 p. 2785 - 2788
