反应条件
1: NiCl2*2H2O; tetrabutylammomium bromide; potassium hydroxide / 12 h / 110 °C / Inert atmosphere
2: hydrogen bromide / 4 h / Inert atmosphere; Reflux
3: potassium carbonate; potassium iodide / acetonitrile / Inert atmosphere; Reflux
4: stannous chloride-dihydrate; ethanol / 1 h / 70 °C / Inert atmosphere
View Scheme
参考文献
Li, Jie; Pei, Shuchen; Zhu, Yingxi; Wu, Jianbo; Chen, Yin; Zhang, Weiyu; Wu, Yong
Letters in Drug Design and Discovery, 2012 , vol. 9, # 4 p. 379 - 388