2,2,2-三氟乙基三氟甲烷磺酸酯合成路线 （共 31 条）
反应条件
trifluoromethanesulfonic acid anhydride in nitrogen
参考文献
Hitachi Chemical Company Ltd.
Patent: US5382687 A1, 1995 ;
参考文献
Tsushima; Kawada; Ishihara; Uchida; Shiratori; Higaki; Hirata
Tetrahedron, 1988 , vol. 44, # 17 p. 5375 - 5387
反应条件
pyridine in dichloromethane T=0°C; 0.416667 h;
参考文献
EP1767526 A1, ;
Page/Page column 26 ;
反应条件
potassium carbonate in xylene T=25°C; 1.2 h; Inert atmosphere; Product distribution / selectivity;
参考文献
Metz, François
Patent: US2011/190542 A1, 2011 ;
Location in patent: Page/Page column 4 ;
反应条件
trifluoromethanesulfonic acid anhydride; N-ethyl-N,N-diisopropylamine in dichloromethane
反应条件
1: 2,2,2-trifluoroethanol With sodium hydride in diethyl ether T=20°C; 1 h; 2: trifluoromethane sulfonylchloride in diethyl ether T=20°C; 1 h;
参考文献
Murata, Junji; Tamura, Masanori; Sekiya, Akira
Journal of Fluorine Chemistry, 2002 , vol. 113, # 1 p. 97 - 100
参考文献
Gmelin Handbook: F: PerFHalOrg.2, 1.3.4, page 137 - 166
反应条件
triethylamine; tetra-n-propylammonium bromide in water T=0 - 2°C; 3.2 h; Product distribution / selectivity;
参考文献
Central Glass Co., Ltd
Patent: JP2005/314356 A, 2005 ;
Location in patent: Page/Page column 9-10; 13 ;
反应条件
potassium carbonate; tetra-n-propylammonium bromide in water T=10.2 - 23.3°C; 4 - 7 h; Product distribution / selectivity;
参考文献
JP2005/314356 A, ;
Page/Page column 11; 13 ;
反应条件
potassium carbonate; triethylamine in water T=13.8 - 21°C; 4 - 5.5 h; Product distribution / selectivity;
参考文献
JP2005/314356 A, ;
Page/Page column 11-13 ;
