5-(异唑-5-基)噻吩-2-磺酰氯合成路线 (共 6 条)
反应条件
trichlorophosphate T=120°C; 2 h;
参考文献
Papet; Marsura
Synthesis, 1993 , # 5 p. 478 - 481
反应条件
potassium carbonate
Methylation;
参考文献
Nugent, Richard A.; Dunn, Colin J.; Staite, Nigel D.; Murphy, Michael J.; Schlachter, Stephen T.; Aspar, Danielle G.; Shields, Sharon K.; Galinet, Louise A.
Phosphorus, Sulfur and Silicon and Related Elements, 1996 , vol. 109, # 1-4 p. 229 - 232
反应条件
1: 87 percent / phosphorus pentachloride, phosphoryl chloride / 3 h / Heating
2: sodium hydroxide / ethanol / 2 h / Heating
View Scheme
参考文献
Brown; Cowden; Lan; Mori
Australian Journal of Chemistry, 1984 , vol. 37, # 1 p. 155 - 163
反应条件
1: 87 percent / phosphorus pentachloride, phosphoryl chloride / 3 h / Heating
2: 3 h / Heating
View Scheme
参考文献
Brown; Cowden; Lan; Mori
Australian Journal of Chemistry, 1984 , vol. 37, # 1 p. 155 - 163
反应条件
1: 87 percent / phosphorus pentachloride, phosphoryl chloride / 3 h / Heating
2: potassium t-butoxide / 1.5 h / Heating
View Scheme
参考文献
Brown; Cowden; Lan; Mori
Australian Journal of Chemistry, 1984 , vol. 37, # 1 p. 155 - 163
反应条件
ueber 4-Chlor-2-methyl-6-phenyl-pyrimidin;
参考文献
Russell
Journal of the Chemical Society, 1954 , p. 2951,2952