3-三甲基硅氧基-2-丁烯酸甲酯合成路线 (共 17 条)
反应条件
triethylamine in hexane T=20°C; 18 h;
参考文献
Kimura, Masanari; Ezoe, Akihiro; Mori, Masahiko; Iwata, Keisuke; Tamaru, Yoshinao
Journal of the American Chemical Society, 2006 , vol. 128, # 26 p. 8559 - 8568
反应条件
chloro-trimethyl-silane; triethylamine in benzene
参考文献
Organix, Inc.; President and Fellows of Harvard College
Patent: US5770180 A1, 1998 ;
US 5770180 A
反应条件
triethylamine T=20°C; 0.583333 h;
参考文献
Aizpurua, Jesus Mari; Palomo, Claudio
Synthesis, 1982 , # 4 p. 280 - 281
参考文献
Synthesis, , p. 722 - 724
反应条件
1: petroleum ether View Scheme
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 40, # 1 p. 97 - 104,88 - 93
参考文献
Liebigs Annalen der Chemie, , # 7 p. 1237 - 1248
反应条件
chloro-trimethyl-silane
参考文献
Organic Mass Spectrometry, , vol. 22, p. 486 - 492
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 40, # 1 p. 97 - 104,88 - 93
反应条件
1) ether, 0 deg C, 2 h, 2) heating; Yield given. Multistep reaction;
参考文献
Zeitschrift fuer Chemie (Stuttgart, Germany), , vol. 28, # 11 p. 409 - 410
反应条件
0.1 h; Ambient temperaturevar.: DMF, 5 min.;
参考文献
Veysoglu, Tarik; Mitscher, Lester A.
Tetrahedron Letters, 1981 , vol. 22, # 14 p. 1303 - 1306