3-三甲基硅氧基-2-丁烯酸甲酯合成路线 （共 17 条）
反应条件
in nitromethane T=50°C; 4 h;
参考文献
Stahl, Ingfried
Chemische Berichte, 1985 , vol. 118, # 12 p. 4857 - 4868
反应条件
in nitromethane 18 h; Ambient temperature;
参考文献
Stahl, Ingfried
Chemische Berichte, 1985 , vol. 118, # 12 p. 4857 - 4868
反应条件
1: 93 percent / LDA / tetrahydrofuran / 0.03 h / -78 °C View Scheme
参考文献
Brownbridge, P.; Chan, T. H.; Brook, M. A.; Kang, G. J.
Canadian Journal of Chemistry, 1983 , vol. 61, p. 688 - 693
反应条件
1: (i) LDA, TMEDA, THF, (ii) /BRN= 1209232/ 2: Br2 View Scheme
参考文献
Chan,T.H.; Brownbridge,P.
Journal of the Chemical Society, Chemical Communications, 1979 , p. 578 - 579
反应条件
1: 93 percent / LDA / tetrahydrofuran / 0.03 h / -78 °C 2: 30 percent / diethyl ether / 4 h / -78 °C View Scheme
参考文献
Chan,T.H.; Brownbridge,P.
Journal of the Chemical Society, Chemical Communications, 1979 , p. 578 - 579
反应条件
n-butyllithium; chloro-trimethyl-silane; N,N,N',N,-tetramethylethylenediamine; diisopropylamine in tetrahydrofuran
参考文献
Organix, Inc.; President and Fellows of Harvard College
Patent: US5770180 A1, 1998 ;
US 5770180 A
反应条件
(i) LDA, THF, (ii) /BRN= 1209232/; Multistep reaction;
参考文献
Am Ende, Christopher W.; Zhou, Zhou; Parker, Kathlyn A.
Journal of the American Chemical Society, 2013 , vol. 135, # 2 p. 582 - 585
