Smith, Catherine J.; Tsang, Melanie W.S.; Holmes, Andrew B.; Danheiser, Rick L.; Tester, Jefferson W.
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 20 p. 3767 - 3781
PdCl(C6H4CH2CH2NH2)(P(C(CH3)3)2(C6H4C6H2(CH(CH3)2)3)); sodium t-butanolate in tetrahydrofuran; tert-butyl alcohol
T=20°C; 2 h;
参考文献
Fors, Brett P.; Watson, Donald A.; Biscoe, Mark R.; Buchwald, Stephen L.
Journal of the American Chemical Society, 2008 , vol. 130, # 41 p. 13552 - 13554
1: With bis(η3-allyl-μ-chloropalladium(II)); cesium hydroxide monohydrate; tri-cyclo-hexyl-phosphine in anhydrous xylene
24 h; RefluxInert atmosphere;
2: With formic acid; sodium cyanoborohydride in ethanol; water
T=25°C; 2 h; Further stages;
