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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-氯苯甲醚
合成路线
（共 685 条）
623-12-1
4-氯苯甲醚
→
反应条件
82020-51-7
反应条件
chlorosulphuric acid; chloroform beim Behandeln der Reaktionsloesung mit Ammoniumcarbonat;
参考文献
Huntress; Carten
Journal of the American Chemical Society, 1940 , vol. 62, p. 603
6165-69-1
3-噻吩硼酸
+
623-12-1
4-氯苯甲醚
→
反应条件
82437-75-0
反应条件
potassium phosphate; N,N'-bis-[2,4,6-tri(3,3,3-trifluoropropyl)phenyl]-4,5-dihydroimidazolium chloride; palladium diacetate in tetrahydrofuran; water Suzuki-Miyaura cross-coupling; 12 h; Inert atmosphereReflux;
参考文献
Liu, Taoping; Zhao, Xiaoming; Shen, Qilong; Lu, Long
Tetrahedron, 2012 , vol. 68, # 32 p. 6535 - 6547
17249-80-8
3-氯噻吩
+
623-12-1
4-氯苯甲醚
→
反应条件
82437-75-0
反应条件
1: 1-methoxy-4-chlorobenzene With tetrahydroxydiboron; ethanol; (X-phos)palladium(II) phenethylamine chloride; potassium acetate; sodium t-butanolate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl T=80°C; 2 h; Inert atmosphere; 2: thien-3-yl chloride With potassium carbonate in ethanol; water T=80°C; Suzuki-Miyaura reaction; 15 h; Inert atmosphere;
参考文献
Molander, Gary A.; Trice, Sarah L. J.; Dreher, Spencer D.
Journal of the American Chemical Society, 2010 , vol. 132, # 50 p. 17701 - 17703
188290-36-0
+
623-12-1
4-氯苯甲醚
→
反应条件
82437-75-0
+
42545-43-7
2-(4-甲氧苯基)噻吩
反应条件
in water; acetonitrile Photolysis; Product distribution; Further Variations:Solvents;
参考文献
Manet, Ilse; Monti, Sandra; Grabner, Gottfried; Protti, Stefano; Dondi, Daniele; Dichiarante, Valentina; Fagnoni, Maurizio; Albini, Angelo
Chemistry - A European Journal, 2008 , vol. 14, # 3 p. 1029 - 1039
188290-36-0
+
623-12-1
4-氯苯甲醚
→
反应条件
82437-75-0
+
42545-43-7
2-(4-甲氧苯基)噻吩
+
100-66-3
苯甲醚
反应条件
in water; acetonitrile Photolysis; Product distribution; Further Variations:Solvents;
参考文献
Manet, Ilse; Monti, Sandra; Grabner, Gottfried; Protti, Stefano; Dondi, Daniele; Dichiarante, Valentina; Fagnoni, Maurizio; Albini, Angelo
Chemistry - A European Journal, 2008 , vol. 14, # 3 p. 1029 - 1039
623-12-1
4-氯苯甲醚
+
611-21-2
N-甲基-邻甲基苯胺
→
反应条件
82463-33-0
反应条件
sodium t-butanolate; SK-CC02-A in 1,4-dioxane T=110°C; Buchwald-Hartwig amination; 2 h;
参考文献
Nettekoven, Ulrike; Naud, Frederic; Schnyder, Anita; Blaser, Hans-Ulrich
Synlett, 2004 , # 14 p. 2549 - 2552
623-12-1
4-氯苯甲醚
→
反应条件
82938-20-3
1-(4-甲氧基苯基)-3-甲基-1-丁酮
反应条件
pyrrolidine; CataCXium POMetB; bis(dibenzylideneacetone)-palladium(0) in N,N-dimethyl acetamide T=140°C; 4 h; Inert atmosphereMolecular sieve;
参考文献
Colbon, Paul; Ruan, Jiwu; Purdie, Mark; Xiao, Jianliang
Organic Letters, 2010 , vol. 12, # 16 p. 3670 - 3673
623-12-1
4-氯苯甲醚
→
反应条件
830345-57-8
反应条件
potassium fluoride; palladium diacetate; potassium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl; dicyclohexyl(2',6'-diisopropoxy-[1,1'-biphenyl]-2-yl)phosphine in water; toluene T=80°C; Suzuki-Miyaura cross-coupling; 24 h; Inert atmosphere;
参考文献
Molander, Gary A.; Sandrock, Deidre L.
Organic Letters, 2009 , vol. 11, # 11 p. 2369 - 2372
623-12-1
4-氯苯甲醚
+
53317-09-2
B-苄基-9-硼杂双环[3.3.1]壬烷
→
反应条件
834-14-0
4 -甲氧基二苯基甲烷
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; palladium diacetate; potassium phosphate in tetrahydrofuran T=60°C; Suzuki-Miyaura reaction; 16 h;
参考文献
Flaherty, Alice; Trunkfield, Amy; Barton, William
Organic Letters, 2005 , vol. 7, # 22 p. 4975 - 4978
623-12-1
4-氯苯甲醚
+
62673-31-8
苄基溴化锌
→
反应条件
834-14-0
4 -甲氧基二苯基甲烷
反应条件
(CH3CON2C3H(CF3)2O)Ni(II)(tris(4-dimethylamino)pyridine) in tetrahydrofuran T=70°C; 24 h; Inert atmosphere;
参考文献
Someya, Chika I.; Inoue, Shigeyoshi; Krackl, Sebastian; Irran, Elisabeth; Enthaler, Stephan
European Journal of Inorganic Chemistry, 2012 , # 8 p. 1269 - 1277
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