sodium; tert-butyl alcohol in diethyl ether; ammonia
Irradiation (UV/VIS); N2-atmosphere; addn. of Na to Sn-compd. (in liquid NH3), addn. of chloroanisole (in Et2O), irradiation (350 nm, 60 min), addn. of slight excess Na and then t-BuOH, addn. of slight excess PhCl, irradiation for 60 min; addn. of excess NH4NO3 and Et2O, evapn. of NH3, water addn., extn. of aq. layer (Et2O), drying of combined org. layers (Na2SO4), distn. (160-170°C/0.5 Torr);
参考文献
Yammal, Carlos C.; Podesta, Julio C.; Rossi, Roberto A.
Journal of Organometallic Chemistry, 1996 , vol. 509, # 1 p. 1 - 8
