反应条件
sodium; tert-butyl alcohol in ammonia
Irradiation (UV/VIS); N2-atmosphere; portionwise addn. of Na to Sn-compd., standing for 20-30 min, addn. of t-BuOH and chloroanisole, irradiation (350 nm, 60 min); addn. of excess NH4NO3 and Et2O, evapn. of NH3, water addn., extn. of aq. layer (Et2O), drying of combined org. layers (Na2SO4), TLC (SiO2, petroleum ether);
参考文献
Yammal, Carlos C.; Podesta, Julio C.; Rossi, Roberto A.
Journal of Organometallic Chemistry, 1996 , vol. 509, # 1 p. 1 - 8