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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-氯苯甲醚
合成路线
（共 685 条）
623-12-1
4-氯苯甲醚
+
849062-15-3
3-丁氧基-2,6-二氟苯基硼酸
+
5720-06-9
2-甲氧基苯基硼酸
→
反应条件
反应条件
potassium phosphate; 2nd generation X-Phos precatalyst in tetrahydrofuran; water T=20°C; Suzuki-Miyaura cross-coupling; 0.5 h; Inert atmosphere;
参考文献
Kinzel, Tom; Zhang, Yong; Buchwald, Stephen L.
Journal of the American Chemical Society, 2010 , vol. 132, # 40 p. 14073 - 14075
623-12-1
4-氯苯甲醚
+
1765-93-1
4-氟苯硼酸
+
5720-06-9
2-甲氧基苯基硼酸
→
反应条件
450-39-5
+
49602-47-3
2,4-二甲氧基联苯
反应条件
potassium phosphate; 2nd generation X-Phos precatalyst in tetrahydrofuran; water T=20°C; Suzuki-Miyaura cross-coupling; 0.5 h; Inert atmosphere;
参考文献
Kinzel, Tom; Zhang, Yong; Buchwald, Stephen L.
Journal of the American Chemical Society, 2010 , vol. 132, # 40 p. 14073 - 14075
623-12-1
4-氯苯甲醚
+
1993-03-9
2-氟苯硼酸
+
5720-06-9
2-甲氧基苯基硼酸
→
反应条件
49602-47-3
2,4-二甲氧基联苯
+
72093-47-1
反应条件
potassium phosphate; 2nd generation X-Phos precatalyst in tetrahydrofuran; water T=20°C; Suzuki-Miyaura cross-coupling; 0.5 h; Inert atmosphere;
参考文献
Kinzel, Tom; Zhang, Yong; Buchwald, Stephen L.
Journal of the American Chemical Society, 2010 , vol. 132, # 40 p. 14073 - 14075
623-12-1
4-氯苯甲醚
+
768-35-4
3-氟苯基硼酸
+
5720-06-9
2-甲氧基苯基硼酸
→
反应条件
49602-47-3
2,4-二甲氧基联苯
+
72093-48-2
反应条件
potassium phosphate; 2nd generation X-Phos precatalyst in tetrahydrofuran; water T=20°C; Suzuki-Miyaura cross-coupling; 0.5 h; Inert atmosphere;
参考文献
Kinzel, Tom; Zhang, Yong; Buchwald, Stephen L.
Journal of the American Chemical Society, 2010 , vol. 132, # 40 p. 14073 - 14075
623-12-1
4-氯苯甲醚
+
5720-06-9
2-甲氧基苯基硼酸
+
162101-25-9
→
反应条件
717101-32-1
+
49602-47-3
2,4-二甲氧基联苯
反应条件
potassium phosphate; 2nd generation X-Phos precatalyst in tetrahydrofuran; water T=20°C; Suzuki-Miyaura cross-coupling; 0.5 h; Inert atmosphere;
参考文献
Kinzel, Tom; Zhang, Yong; Buchwald, Stephen L.
Journal of the American Chemical Society, 2010 , vol. 132, # 40 p. 14073 - 14075
623-12-1
4-氯苯甲醚
+
5720-06-9
2-甲氧基苯基硼酸
+
182482-25-3
→
反应条件
1206164-33-1
+
49602-47-3
2,4-二甲氧基联苯
反应条件
potassium phosphate; 2nd generation X-Phos precatalyst in tetrahydrofuran; water T=20°C; Suzuki-Miyaura cross-coupling; 0.5 h; Inert atmosphere;
参考文献
Kinzel, Tom; Zhang, Yong; Buchwald, Stephen L.
Journal of the American Chemical Society, 2010 , vol. 132, # 40 p. 14073 - 14075
623-12-1
4-氯苯甲醚
+
5720-06-9
2-甲氧基苯基硼酸
+
98-80-6
→
反应条件
613-37-6
+
49602-47-3
2,4-二甲氧基联苯
反应条件
potassium phosphate; 2nd generation X-Phos precatalyst in tetrahydrofuran; water T=20°C; Suzuki-Miyaura cross-coupling; 0.5 h; Inert atmosphere;
参考文献
Kinzel, Tom; Zhang, Yong; Buchwald, Stephen L.
Journal of the American Chemical Society, 2010 , vol. 132, # 40 p. 14073 - 14075
623-12-1
4-氯苯甲醚
+
5720-06-9
2-甲氧基苯基硼酸
→
反应条件
1206164-29-5
+
49602-47-3
2,4-二甲氧基联苯
反应条件
potassium phosphate; 2nd generation X-Phos precatalyst in tetrahydrofuran; water T=20°C; Suzuki-Miyaura cross-coupling; 0.5 h; Inert atmosphere;
参考文献
Kinzel, Tom; Zhang, Yong; Buchwald, Stephen L.
Journal of the American Chemical Society, 2010 , vol. 132, # 40 p. 14073 - 14075
623-12-1
4-氯苯甲醚
+
201813-47-0
→
反应条件
5034-76-4
反应条件
caesium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl; tris(dibenzylideneacetone)dipalladium (0) in acetonitrile T=120°C; 5 h;
参考文献
Cacchi, Sandro; Fabrizi, Giancarlo; Goggiamani, Antonella
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 10-11 p. 1301 - 1305
623-12-1
4-氯苯甲醚
+
927-74-2
→
反应条件
52999-15-2
反应条件
cesium hydroxide; C23H37O3PS; palladium diacetate in water; acetonitrile T=23°C; Sonogashira coupling; Inert atmosphere;
参考文献
Brown, William S.; Boykin, D'Ariel D.; M. Quentin Sonnier Jr.; William D. Clark; Brown, Fallon V.; Shaughnessy, Kevin H.
Synthesis, 2008 , # 12 art. no. C00208SS, p. 1965 - 1970
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