in tetrahydrofuran A mixt. of BrCH2C6H4CH2Br and Na(MO(cp)(CO)3) in THF is stirred at roomtemp. for 1.5 h.; The soln. is filtered to remove NaBr, concd. in vacuo and treated with methanol to give yellow crystals of (Mo(cp)(CO)3)CH2C6H4CH2((CO)3(cp)Mo);
samarium diiodide in tetrahydrofuran 1 h; Ambient temperature; Further byproducts given;
参考文献
Takahashi, Senji; Mori, Nobuo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 8 p. 2029 - 2032
samarium diiodide in tetrahydrofuran 0.166667 h; Ambient temperature; Further byproducts given;
参考文献
Takahashi, Senji; Mori, Nobuo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 8 p. 2029 - 2032
samarium diiodide in tetrahydrofuran 1 h; Ambient temperature; Further byproducts given;
参考文献
Takahashi, Senji; Mori, Nobuo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 8 p. 2029 - 2032