1,4-二(溴甲基)苯合成路线 （共 136 条）
反应条件
1,5-bis(2-(2-methoxyethoxy)ethoxy)naphthalene in N,N-dimethyl-formamide P=9000720 Torr; 72 h; Ambient temperature;
参考文献
Asakawa, Masumi; Dehaen, Wim; L'abbe, Gerrit; Menzer, Stephan; Nouwen, Jan; Raymo, Francisco M.; Stoddart, J. Fraser; Williams, David J.
Journal of Organic Chemistry, 1996 , vol. 61, # 26 p. 9591 - 9595
反应条件
1: in N,N-dimethyl-formamide T=20°C; 120 h; 2: With NH4PF6; water
参考文献
European Journal of Organic Chemistry, , # 35 p. 6798 - 6803
反应条件
1: aq. NH4PF6 / acetonitrile / Heating 2: aq. NH4PF6 / acetonitrile / Heating View Scheme
参考文献
Alvaro, Mercedes; Ferrer, Belen; Fornes, Vicente; Garcia, Hermenegildo; Scaiano
Journal of Physical Chemistry B, 2002 , vol. 106, # 26 p. 6815 - 6820
反应条件
1: K2CO3 / dimethylformamide / Ambient temperature 2: K2CO3 / dimethylformamide / Ambient temperature View Scheme
参考文献
Baker,B.R.; Ashton,W.T.
Journal of Medicinal Chemistry, 1970 , vol. 13, # 6 p. 1149 - 1154
反应条件
potassium carbonate in N,N-dimethyl-formamide Ambient temperature;
参考文献
Baker,B.R.; Ashton,W.T.
Journal of Medicinal Chemistry, 1970 , vol. 13, # 6 p. 1149 - 1154
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydroxide in toluene T=60°C; 1 h;
参考文献
Argent, Stephen P.; Adams, Harry; Riis-Johannessen, Thomas; Jeffery, John C.; Harding, Lindsay P.; Ward, Michael D.
Journal of the American Chemical Society, 2006 , vol. 128, # 1 p. 72 - 73
反应条件
T=185°C; Arbusov reaction; 6 h;
参考文献
Plater, M. John; Jackson, Toby
Tetrahedron, 2003 , vol. 59, # 25 p. 4673 - 4685
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 111, p. 162
反应条件
5 h; RefluxInert atmosphereSchlenk technique;
参考文献
Wu, Tong; Lin, Yue-Jian; Jin, Guo-Xin
Dalton Transactions, 2014 , vol. 43, # 6 p. 2356 - 2360
反应条件
ammonium hydroxide; iodine T=20 - 60°C; 4 h; Time;
参考文献
Tsuchiya, Daisuke; Kawagoe, Yuhsuke; Moriyama, Katsuhiko; Togo, Hideo
Organic Letters, 2013 , vol. 15, # 16 p. 4194 - 4197
