反应条件
1.1: sodium tetrahydroborate / methanol / 1 h / 20 °C
2.1: tetrahydrofuran / 0.17 h / 0 °C / |Inert atmosphere; |Sealed tube
2.2: 0 - 20 °C / |Inert atmosphere; |Sealed tube
2.3: 0 - 20 °C / |Inert atmosphere; |Sealed tube
3.1: oxoammonium salt; silica gel / dichloromethane / 24 h / 20 °C / |Acidic conditions
4.1: oxoammonium salt; 2,6-dimethylpyridine / dichloromethane / 20 °C / |Sealed tube
View Scheme
参考文献
Kelly, Christopher B.; Mercadante, Michael A.; Hamlin, Trevor A.; Fletcher, Madison H.; Leadbeater, Nicholas E.
Journal of Organic Chemistry, 2012 , vol. 77, # 18 p. 8131 - 8141
