3-(2-呋喃基)丙烯醛合成路线 （共 28 条）
反应条件
hydrogen; nickel in ethanol
T=80°C; P=76000.1 Torr;
参考文献
Klochkova, I. N.; Kulikova, L. K.; Krasheninnikova, M. K.; Noritsina, M. V.
Pharmaceutical Chemistry Journal, 1983 , vol. 17, # 8 p. 553 - 556
Khimiko-Farmatsevticheskii Zhurnal, 1983 , vol. 17, # 8 p. 931 - 934
反应条件
1: 50 percent / H2 / Raney nickel / ethanol / 80 °C / 76000.1 Torr
2: 40 percent / H2, aq. HCl / Raney nickel/1percent Hg / dioxane / 120 °C / 38000 Torr
View Scheme
参考文献
Klochkova, I. N.; Kulikova, L. K.; Krasheninnikova, M. K.; Noritsina, M. V.
Pharmaceutical Chemistry Journal, 1983 , vol. 17, # 8 p. 553 - 556
Khimiko-Farmatsevticheskii Zhurnal, 1983 , vol. 17, # 8 p. 931 - 934
反应条件
sodium tetrahydroborate in methanol
1 h; Ambient temperature;
参考文献
Iwasaki, Masakazu; Kobayashi, Yoshihiro; Li, Ji-Ping; Matsuzaka, Hiroyuki; Ishii, Youichi; Hidai, Masanobu
Journal of Organic Chemistry, 1991 , vol. 56, # 5 p. 1922 - 1927
反应条件
sodium hydroxide in diethyl ether; water
4 h; Heating;
参考文献
Shapiro, Yu. M.; Smolyakov, V. P.; Kul'nevich, V. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1990 , vol. 26, # 6 p. 617 - 620
Khimiya Geterotsiklicheskikh Soedinenii, 1990 , # 6 p. 741 - 744
反应条件
bis(cyclopentadienyl)titanium dichloride; triethyl amine hydrochloride; zinc in dichloromethane
T=20°C; 1 h;
参考文献
Naud, Sebastien; MacNaughton, Sarah J.; Dyson, Bryony S.; Woollaston, Daniel J.; Dallimore, Jonathan W. P.; Robertson, Jeremy
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 17 p. 3506 - 3518
反应条件
hydrogen; lt;Pd-PARgt; in isopropyl alcohol
T=25°C; P=750.06 Torr; effect of temperature, solvent, various additives; other catalysts; Product distribution;
参考文献
Shebaldova; Safronova; Kravtsova
Russian Journal of General Chemistry, 1996 , vol. 66, # 1 p. 109 - 112
反应条件
4 A molecular sieve in benzene
T=80°C; 6 h;
参考文献
Iovel; Golomba; Belyakov; Popelis; Gaukhman; Lukevics
Chemistry of Heterocyclic Compounds, 2003 , vol. 39, # 3 p. 318 - 327
反应条件
ethanol; nickel; acetic acid
T=190°C; P=61782.7 Torr; Hydrogenation;
参考文献
Russell et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 4543,4545, 4546
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Vranjican et al.
Arhiv za Kemiju, 1953 , vol. 25, p. 81,83
Chem.Abstr., 1955 , p. 2419
