3-甲氧基-1,2-丙二醇合成路线 (共 36 条)
反应条件
H3[PW12O40]; water in acetonitrile T=20°C; 2 h;
参考文献
Vanlaldinpuia, Khiangte; Bez, Ghanashyam
Tetrahedron Letters, 2011 , vol. 52, # 29 p. 3759 - 3764
反应条件
perchloric acid in water T=80°C; 24 h;
参考文献
Ribelin, Timothy; Katz, Christopher E.; English, Donna G.; Smith, Sherriel; Manukyan, Anna K.; Day, Victor W.; Neuenswander, Benjamin; Poutsma, Jennifer L.; Aube, Jeffrey
Angewandte Chemie - International Edition, 2008 , vol. 47, # 33 p. 6233 - 6235
反应条件
RuHCl(CO)(bis-(2-diphenylphosphinoethyl)amine); potassium tert-butylate; hydrogen in tetrahydrofuran T=140°C; 4 h; Autoclave;
参考文献
Angewandte Chemie - International Edition, , vol. 51, # 52 p. 13041 - 13045
Angew. Chem., , vol. 124, # 52
反应条件
1: glycerol With sodium hydroxide in water T=120°C; 2: dimethyl sulfate in water T=120 - 125°C;
参考文献
Chen, Jin; Du, Xiaohua
Synthetic Communications, 2011 , vol. 41, # 9 p. 1376 - 1380
反应条件
potassium acetate; acetic acid T=165°C; unter Druck und Kochen des Reaktionsprodukts mit waessrig-alkoholischer Salzsaeure;
参考文献
Journal of the American Chemical Society, , vol. 51, p. 1946
反应条件
trifluorormethanesulfonic acid; [cpRu(CH3CN)(bipy)](OTf); hydrogen in sulfolane T=200°C; P=25877.6 Torr; 3.5 h; Autoclave;
参考文献
Green Chemistry, , vol. 13, # 2 p. 357 - 366
反应条件
trifluorormethanesulfonic acid; aqua(2,2'-bipyridine)(η5-pentamethylcyclopentadienyl)ruthenium(II) triflate; hydrogen in sulfolane T=200°C; P=25877.6 Torr; 3.5 h; Autoclave;
参考文献
Green Chemistry, , vol. 13, # 2 p. 357 - 366
反应条件
in methanol 0.5 h; Heating;
参考文献
Birkofer, Leonhard; Stuhl, Oskar
Journal of Organometallic Chemistry, 1980 , vol. 187, # 1 p. 21 - 29
反应条件
sodium hydroxide T=90 - 100°C;
参考文献
Koshchii
Russian Journal of Applied Chemistry, 2002 , vol. 75, # 9 p. 1434 - 1437
反应条件
carbon tetrabromide Ring cleavage; ether cleavage; 4 h; Heating;
参考文献
Yadav; Reddy, B. V. Subba
Chemistry Letters, 2000 , # 5 p. 566 - 567