3-甲氧基-1,2-丙二醇合成路线 （共 36 条）
反应条件
sodium hydride in tetrahydrofuran
24 h; Heating;
参考文献
Nakatsuji, Yohji; Nakamura, Tetsuya; Okahara, Mitsuo; Dishong, Dennis M.; Gokel, George W.
Journal of Organic Chemistry, 1983 , vol. 48, # 8 p. 1237 - 1242
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Dishong, Dennis M.; Diamond, Craig J.; Cinoman, Michael I.; Gokel, Geoge W.
Journal of the American Chemical Society, 1983 , vol. 105, # 3 p. 586 - 593
反应条件
diethyl ether; 2,3-dimethyl aniline; phosphorus trichoride
参考文献
Arbusow; Soroastrowa; Rispoloshenski
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1948 , p. 208
Chem.Abstr., 1948 , p. 4934
反应条件
chloroform; phosphorus tribromide; phosphorus pentabromide
参考文献
Wwedenskii
Ukrainskii Khimicheskii Zhurnal (Russian Edition), 1959 , vol. 25, p. 203
Chem.Abstr., 1959 , p. 21615
反应条件
sulfuric acid; water; nitric acid
T=13 - 20°C;
参考文献
Eremenko,L.T.; Korolev,A.M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1977 , vol. 26, # 2 p. 399 - 401
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1977 , vol. 26, # 2 p. 440 - 444
反应条件
oxygen; palladium diacetate; Mn(III) acetylacetonate; potassium bromide in ethyl acetate
T=60°C; P=15001.5 Torr; 20 h; Inert atmosphereAutoclave;
参考文献
Doro, Franco; Winnertz, Patrick; Leitner, Walter; Prokofieva, Angelina; Mueller, Thomas E.
Green Chemistry, 2011 , vol. 13, # 2 p. 292 - 295
反应条件
di(n-butyl)tin oxide; cesium fluoride
1) toluene, 1 h, reflux, 2) DMF, r.t., 44 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Nagashima; Ohno
Chemical and Pharmaceutical Bulletin, 1991 , vol. 39, # 8 p. 1972 - 1982
