1: N-bromosuccinimide
2: benzene / 1.) 20 deg C, 2 h, 2.) 60-70 deg C, 4 h
3: NaOH / diethyl ether / 4 h
4: H2SO4 / aq. ethanol / 2 h
5: 94 percent / CaCl2 / 72 h / Ambient temperature
6: 1.) NaH / 1.) DMSO, 2.) 2 h
7: 93 percent / H2SO4 / H2O / 3 h
8: 52 percent / conc. HCl / diethyl ether / 6 h / 0 °C
View Scheme
参考文献
Landor, Stephen R.; Landor, Phyllis, D.; Kalli, Michael
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2921 - 2926
