反应条件
1.1: O-(2,4-dinitro-phenyl)-hydroxylamine / acetonitrile / 18 h / 40 °C 1.2: 18 h / 20 °C 2.1: dichloromethane / 18 h / 20 °C 3.1: hydrogen bromide; sodium nitrite / water / 0.25 h / 0 °C 3.2: 0.25 h / 50 °C 3.3: pH 5 View Scheme
参考文献
Kendall, Jackie D.; O'Connor, Patrick D.; Marshall, Andrew J.; Frederick, Raphael; Marshall, Elaine S.; Lill, Claire L.; Lee, Woo-Jeong; Kolekar, Sharada; Chao, Mindy; Malik, Alisha; Yu, Shuqiao; Chaussade, Claire; Buchanan, Christina; Rewcastle, Gordon W.; Baguley, Bruce C.; Flanagan, Jack U.; Jamieson, Stephen M.F.; Denny, William A.; Shepherd, Peter R.
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 1 p. 69 - 85