反应条件
1.1: n-butyllithium / tetrahydrofuran / 0.08 h / -78 °C / |Inert atmosphere 1.2: 1 h / -78 °C / |Inert atmosphere 2.1: sodium hydrogencarbonate; hydroquinone / water; dimethyl sulfoxide / 18 h / 23 °C / |Inert atmosphere 3.1: titanium(III) chloride / water; tetrahydrofuran; acetone / 0.17 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Tiruveedhula, V.V.N. Phani Babu; Witzigmann, Christopher M.; Verma, Ranjit; Kabir, M. Shahjahan; Rott, Marc; Schwan, William R.; Medina-Bielski, Sara; Lane, Michelle; Close, William; Polanowski, Rebecca L.; Sherman, David; Monte, Aaron; Deschamps, Jeffrey R.; Cook, James M.
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 24 p. 7830 - 7840