n-butyllithium; diisopropylamine in tetrahydrofuran
T=-78°C; 1 h;
参考文献
Crimmins, Michael T.; Pace, Jennifer M.; Nantermet, Philippe G.; Kim-Meade, Agnes S.; Thomas, James B.; Watterson, Scott H.; Wagman, Allan S.
Journal of the American Chemical Society, 2000 , vol. 122, # 35 p. 8453 - 8463
in N,N-dimethyl-formamide
T=20°C; 0.333333 h; optical yield given as percent destereoselective reaction;
参考文献
Downey, C. Wade; Craciun, Smaranda; Neferu, Ana M.; Vivelo, Christina A.; Mueller, Carly J.; Southall, Brian C.; Corsi, Stephanie; Etchill, Eric W.; Sault, Ryan J.
Tetrahedron Letters, 2012 , vol. 53, # 43 p. 5763 - 5765
ammonium hydroxide; zinc in 1,4-dioxane
Michael Addition; 24 h; Schlenk techniqueRefluxInert atmosphere; Overall yield = 83 percent; diastereoselective reaction;
参考文献
Loren Nunes, Vanessa; De Oliveira, Ingryd Cristina; Soares Do Rego Barros, Olga
European Journal of Organic Chemistry, 2014 , vol. 2014, # 7 p. 1525 - 1530