1: 22.2 g / sodium hyrdoxide, hydrogen sulphide / aq. ethanol / 2 h / 0 °C
2: 6.24 g / H2O; acetone / 0.5 h / 0 °C
View Scheme
参考文献
Branch, Clive L.; Pearson, Michael J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1097 - 1100
1: With copper(l) iodide; N-ethyl-N,N-diisopropylamine; phenyl chloroformate in acetonitrile
T=20°C; Inert atmosphere;
2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in acetonitrile
1 h; Heating;
参考文献
Beveridge, Ramsay E.; Arndtsen, Bruce A.
Synthesis, 2010 , # 6 art. no. M05809SS, p. 1000 - 1008