反应条件
1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.25 h / -78 °C / |Inert atmosphere
1.2: 0.5 h / -78 °C / |Inert atmosphere
2.1: lithium perchlorate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1.5 h / 20 - 40 °C / |Inert atmosphere
View Scheme
参考文献
Downey, C. Wade; Craciun, Smaranda; Vivelo, Christina A.; Neferu, Ana M.; Mueller, Carly J.; Corsi, Stephanie
Tetrahedron Letters, 2012 , vol. 53, # 43 p. 5766 - 5768