反应条件
hydrogen in chloroform dry solvents; degassing mixt. of Mo-compd./EtO2CCN dissolved in CHCl3, placing under H2 (600 Torr at -196°C), stirring at room temperature, frozing mixt. at -196°C, addn. of acid, stirring under H2 (600 Torr), total react. time 4 days; removal of solvent under reduced pressure, chromy. (Al2O3, MeCN/CHCl3 80:20), evapn. of solvent under reduced pressure, dissolving (MeCN), pptn. by addn. of Et2O, filtration, drying in vac.; elem. anal.;
参考文献
Organometallics, , vol. 9, p. 1607 - 1617
