O-乙基 S-甲基二硫代碳酸酯合成路线 (共 25 条)
反应条件
in acetone
T=0 - 20°C;
参考文献
Kakaei, Saeed; Chen, Ning; Xu, Jiaxi
Tetrahedron, 2013 , vol. 69, # 1 p. 302 - 309
反应条件
1: carbon disulfide; ethanol in dimethyl sulfoxide
T=20°C; 0.333333 h;
2: With N-benzyl-trimethylammonium hydroxide in dimethyl sulfoxide
T=20°C; 1 h;
3: methyl iodide in dimethyl sulfoxide
T=20°C; 2.5 h;
参考文献
Chaturvedi, Devdutt; Ray, Suprabhat
Monatshefte fur Chemie, 2006 , vol. 137, # 9 p. 1219 - 1223
反应条件
18-crown-6 ether in dichloromethane
1 h; Ambient temperature;
参考文献
Chenevert, Robert; Paquin, Robert; Rodrigue, Andre
Synthetic Communications, 1981 , vol. 11, # 10 p. 817 - 822
反应条件
in ethanol; dimethyl sulfoxide
T=0°C;
参考文献
Moussounga, Jacques Emmanuel; Bouquant, James; Chuche, Josselin
Bulletin de la Societe Chimique de France, 1995 , vol. 132, # 2 p. 249 - 258
反应条件
N-butylamine in ethanol
T=0°C; 5 h;
参考文献
Palominos, Mario A.; Santos, Jose G.; Valderrama, Jaime A.; Vega, Juan C.
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 15, p. 245 - 252
参考文献
Palominos, Mario A.; Vega, Juan C.
Phosphorus, Sulfur and Silicon and the Related Elements, 1991 , vol. 61, # 3.4 p. 319 - 324
反应条件
in chloroform-d1
24 h;
参考文献
Palominos, Mario A.; Vega, Juan C.
Phosphorus, Sulfur and Silicon and the Related Elements, 1991 , vol. 61, # 3.4 p. 319 - 324
参考文献
Chancel
Jahresbericht ueber die Fortschritte der Chemie und Verwandter Theile Anderer Wissenschaften, 1850 , p. 470
反应条件
in ethanol
T=0°C; 0.5 h; product distribution depending on the time; Product distribution;
参考文献
Palominos, Mario A.; Santos, Jose G.; Valderrama, Jaime A.; Vega, Juan C.
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 15, p. 245 - 252
反应条件
chlorine in pentane
T=-50 - -30°C;
参考文献
Barany, George; Schroll, Alayne L.; Mott, Andrew W.; Halsrud, David A.
Journal of Organic Chemistry, 1983 , vol. 48, # 24 p. 4750 - 4761