反应条件
1: dimethyl 3-chloropropylboronate With potassium fluoride; (trifluoromethyl)-trimethylsilane in ethylene glycol dimethyl ether T=20°C; 18 h; Inert atmosphere; 2: With chloro-trimethyl-silane in ethylene glycol dimethyl ether T=-20 - -10°C; 0.333333 h; Inert atmosphere; 3: diazoacetic acid ethyl ester With methanol in ethylene glycol dimethyl ether T=-20 - 20°C; 2 h; Inert atmosphere;
参考文献
Elkin, Pavel K.; Levin, Vitalij V.; Dilman, Alexander D.; Struchkova, Marina I.; Belyakov, Pavel A.; Arkhipov, Dmitry E.; Korlyukov, Alexander A.; Tartakovsky, Vladimir A.
Tetrahedron Letters, 2011 , vol. 52, # 41 p. 5259 - 5263
