in neat (no solvent)
byproducts: H3SiCl, (H2SiS)3; compds. condensed into a vessel, reacted at 20°C for 21 days, ratio (H3Si)2S:H2SiCl2 = 2:1; fractional distn., chloro-product not analytically pure;
参考文献
Haas, Alois; Hitze, Reiner; Krueger, Carl; Angermund, Klaus
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1984 , vol. 39, # 7 p. 890 - 896
