N-已酰基-5-溴-7-硝基吲哚合成路线 (共 7 条)
反应条件
sodium nitrate; trifluoroacetic acid 4 h; Ambient temperature;
参考文献
Mortensen, Michael B.; Kamounah, Fadhil S.; Christensen, Jorn B.
Organic Preparations and Procedures International, 1996 , vol. 28, # 1 p. 123 - 125
反应条件
1: Br2; AcOH 2: HNO3; H2SO4 / acetic acid / 6 h / 5 °C View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 48, # 6 p. 817 - 827
反应条件
1: CHCl3 / 1 h / 20 °C 2: Br2; AcOH 3: HNO3; H2SO4 / acetic acid / 6 h / 5 °C View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 48, # 6 p. 817 - 827
反应条件
1: palladium/charcoal; ethanol / Hydrogenation 2: aqueous sulfuric acid; sodium nitrite / Behandeln der erhaltenen Diazoniumsalz-Loesung mit Kaliumjodid und Kupfer-Pulver View Scheme
参考文献
Gall et al.
Journal of Organic Chemistry, 1955 , vol. 20, p. 1538,1541
反应条件
palladium on activated charcoal; ethanol Hydrogenation;
参考文献
Gall et al.
Journal of Organic Chemistry, 1955 , vol. 20, p. 1538,1541
反应条件
sodium hydroxide in methanol Deacetylation; 2 h; Heating;
参考文献
Eisai Co., Ltd.
Patent: US5721246 A1, 1998 ;
反应条件
hydrogenchloride in ethanol; water
参考文献
Kyorin Pharmaceutical Co., Ltd.
Patent: US5242912 A1, 1993 ;