反应条件
1: 2,3-dihydro-5-chloroindole With n-butyllithium in diethyl ether; hexane
T=0 - 20°C; 1 h; Inert atmosphereSchlenk technique;
2: N,N-dimethylcarbamoyl chloride in diethyl ether; hexane
T=0 - 20°C; 14 h; Inert atmosphereSchlenk technique;
参考文献
Jiao, Lin-Yu; Oestreich, Martin
Organic Letters, 2013 , vol. 15, # 20 p. 5374 - 5377