(9ci)-5-甲基-1H-苯并咪唑 3-氧化物合成路线 （共 9 条）
反应条件
T=750°C; P=0.05 - 0.07 Torr;
参考文献
Harvey, Ian W.; McFarlane, Michael D.; Moody, David J.; Smith, David M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 681 - 690
反应条件
sodium tetrahydroborate; palladium on activated charcoal in pyridine
T=35 - 40°C; 0.25 h;
参考文献
Harvey, Ian W.; McFarlane, Michael D.; Moody, David J.; Smith, David M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 681 - 690
反应条件
1: 75 percent / cc. sulphuric acid, ZnCl2 / acetic acid
2: 67 percent / aq. sulphuric acid / acetic acid / 2.5 h / 100 °C
3: 83 percent / HCl / Heating
4: 46 percent / sodium ethoxide / ethanol; dimethylformamide / 2 h
5: 85 percent / cc. HCl / 4 h
6: 72 percent / aq.NH3
View Scheme
参考文献
Harvey, Ian W.; McFarlane, Michael D.; Moody, David J.; Smith, David M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 681 - 690
反应条件
1: 67 percent / aq. sulphuric acid / acetic acid / 2.5 h / 100 °C
2: 83 percent / HCl / Heating
3: 46 percent / sodium ethoxide / ethanol; dimethylformamide / 2 h
4: 85 percent / cc. HCl / 4 h
5: 72 percent / aq.NH3
View Scheme
参考文献
Harvey, Ian W.; McFarlane, Michael D.; Moody, David J.; Smith, David M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 681 - 690
反应条件
1: 83 percent / HCl / Heating
2: 46 percent / sodium ethoxide / ethanol; dimethylformamide / 2 h
3: 85 percent / cc. HCl / 4 h
4: 72 percent / aq.NH3
View Scheme
参考文献
Harvey, Ian W.; McFarlane, Michael D.; Moody, David J.; Smith, David M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 681 - 690
反应条件
1: 46 percent / sodium ethoxide / ethanol; dimethylformamide / 2 h
2: 85 percent / cc. HCl / 4 h
3: 72 percent / aq.NH3
View Scheme
参考文献
Harvey, Ian W.; McFarlane, Michael D.; Moody, David J.; Smith, David M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 681 - 690
反应条件
1: 64 percent / cc. HCl / 4 h
2: 72 percent / aq.NH3
View Scheme
参考文献
Harvey, Ian W.; McFarlane, Michael D.; Moody, David J.; Smith, David M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 681 - 690
反应条件
1: 85 percent / cc. HCl / 4 h
2: 72 percent / aq.NH3
View Scheme
参考文献
Harvey, Ian W.; McFarlane, Michael D.; Moody, David J.; Smith, David M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 681 - 690
反应条件
T=700°C; P=0.01 - 0.02 Torr; Yield given. Yields of byproduct given;
参考文献
Harvey, Ian W.; McFarlane, Michael D.; Moody, David J.; Smith, David M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 681 - 690
