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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
62378-28-3
合成路线
（共 10 条）
5720-06-9
2-甲氧基苯基硼酸
+
246230-86-4
3-碘-2-苯基-苯并呋喃
→
反应条件
62378-28-3
反应条件
triphenylphosphine; cesium fluoride; palladium diacetate in ethylene glycol dimethyl ether T=75°C; Suzuki reaction; 16 h;
参考文献
Colobert, Francoise; Castanet, Anne-Sophie; Abillard, Olivier
European Journal of Organic Chemistry, 2005 , # 15 p. 3334 - 3341
678967-05-0
→
反应条件
62378-28-3
+
753501-20-1
反应条件
1: With NiO2 in acetonitrile T=0°C; 0.666667 h; 2: With toluene-4-sulfonic acid in acetonitrile
参考文献
Fujita, Megumi; Qi, Guizhong; Verkerk, Udo H.; Dzwiniel, Trevor L.; McDonald, Robert; Stryker, Jeffrey M.
Organic Letters, 2004 , vol. 6, # 16 p. 2653 - 2656
536-74-3
苯乙炔
→
反应条件
62378-28-3
反应条件
1.1: nBuLi; B(OMe)3 / hexane; 1,2-dimethoxy-ethane / 3.5 h / -78 - 20 °C 1.2: 89 percent / Pd(PPh3)4 / tetrahydrofuran; 1,2-dimethoxy-ethane / 16 h / Heating 2.1: 80 percent / BCl3; NIS / heptane; CH2Cl2 / 2 h / 20 °C 3.1: 91 percent / CsF; PPh3 / Pd(OAc)2 / 1,2-dimethoxy-ethane / 16 h / 75 °C View Scheme
参考文献
Colobert, Francoise; Castanet, Anne-Sophie; Abillard, Olivier
European Journal of Organic Chemistry, 2005 , # 15 p. 3334 - 3341
529-28-2
2-碘苯甲醚
→
反应条件
62378-28-3
反应条件
1.1: BuLi; B(OMe)3 / 1,2-dimethoxy-ethane; hexane / 1.75 h / -78 - 20 °C 1.2: PPh3 / Pd(OAc)2 / 1,2-dimethoxy-ethane / 4 h / Heating 1.3: 52 percent / BCl3; NIS / CH2Cl2; hexane / 20 °C 2.1: 91 percent / CsF; PPh3 / Pd(OAc)2 / 1,2-dimethoxy-ethane / 16 h / 75 °C View Scheme
参考文献
Colobert, Francoise; Castanet, Anne-Sophie; Abillard, Olivier
European Journal of Organic Chemistry, 2005 , # 15 p. 3334 - 3341
41398-67-8
1-甲氧基-2-苯基乙炔-苯
→
反应条件
62378-28-3
反应条件
1: 80 percent / BCl3; NIS / heptane; CH2Cl2 / 2 h / 20 °C 2: 91 percent / CsF; PPh3 / Pd(OAc)2 / 1,2-dimethoxy-ethane / 16 h / 75 °C View Scheme
参考文献
Colobert, Francoise; Castanet, Anne-Sophie; Abillard, Olivier
European Journal of Organic Chemistry, 2005 , # 15 p. 3334 - 3341
13102-33-5
二(2-甲氧基苯基)甲酮
→
反应条件
62378-28-3
反应条件
1.1: BCl3 / CH2Cl2 / 1.25 h / -65 - 20 °C 2.1: 97 percent / K2CO3 / dimethylsulfoxide / 20 °C 3.1: hydrazine hydrate / butan-1-ol / Heating 4.1: NiO2 / acetonitrile / 0.67 h / 0 °C 4.2: p-TsOH / acetonitrile View Scheme
参考文献
Fujita, Megumi; Qi, Guizhong; Verkerk, Udo H.; Dzwiniel, Trevor L.; McDonald, Robert; Stryker, Jeffrey M.
Organic Letters, 2004 , vol. 6, # 16 p. 2653 - 2656
21147-18-2
→
反应条件
62378-28-3
反应条件
1.1: 97 percent / K2CO3 / dimethylsulfoxide / 20 °C 2.1: hydrazine hydrate / butan-1-ol / Heating 3.1: NiO2 / acetonitrile / 0.67 h / 0 °C 3.2: p-TsOH / acetonitrile View Scheme
参考文献
Fujita, Megumi; Qi, Guizhong; Verkerk, Udo H.; Dzwiniel, Trevor L.; McDonald, Robert; Stryker, Jeffrey M.
Organic Letters, 2004 , vol. 6, # 16 p. 2653 - 2656
678967-04-9
→
反应条件
62378-28-3
反应条件
1.1: hydrazine hydrate / butan-1-ol / Heating 2.1: NiO2 / acetonitrile / 0.67 h / 0 °C 2.2: p-TsOH / acetonitrile View Scheme
参考文献
Fujita, Megumi; Qi, Guizhong; Verkerk, Udo H.; Dzwiniel, Trevor L.; McDonald, Robert; Stryker, Jeffrey M.
Organic Letters, 2004 , vol. 6, # 16 p. 2653 - 2656
62378-32-9
→
反应条件
62378-28-3
反应条件
in benzene 6 h; Irradiation;
参考文献
Suzuki, Tatsuo; Kitamura, Tsugio; Sonoda, Taka-aki; Kobayashi, Shinjiro; Taniguchi, Hiroshi
Journal of Organic Chemistry, 1981 , vol. 46, p. 5324 - 5328
62378-32-9
→
反应条件
62378-28-3
+
62378-39-6
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in dimethyl sulfoxide 4 h; Ambient temperatureIrradiationother reagent, solvent, reaction time; effect of wavelength; Product distribution;
参考文献
Galli, Carlo; Gentili, Patrizia; Guarnieri, Alessandra; Kobayashi, Shinjiro; Rappoport, Zvi
Journal of Organic Chemistry, 1998 , vol. 63, # 25 p. 9292 - 9299
