1-(3-甲氧基苯基)-2-苯基乙酮合成路线 (共 27 条)
反应条件
NiBr2bipy; tetra-n-butylammonium tetrafluoroborate in N,N-dimethyl-formamide
Electrochemical reaction;
参考文献
Dolhem, Eric; Barhdadi, Rachid; Folest, Jean Claude; Nedelec, Jean Yves; Troupel, Michel
Tetrahedron, 2001 , vol. 57, # 3 p. 525 - 529
反应条件
palladium diacetate; 1,4-di(diphenylphosphino)-butane; zinc in 1,4-dioxane
T=100°C; Negishi coupling reaction; 3 h; Inert atmosphere;
参考文献
Wu, Xiao-Feng; Schranck, Johannes; Neumann, Helfried; Beller, Matthias
Chemistry - An Asian Journal, 2012 , vol. 7, # 1 p. 40 - 44
反应条件
1: tetrahydrofuran / -78 °C
2: Jones reagent
View Scheme
参考文献
Wrobel; Millen; Sredy; Dietrich; Gorham; Malamas; Kelly; Bauman; Harrison; Jones; Guinosso; Sestanj
Journal of Medicinal Chemistry, 1991 , vol. 34, # 8 p. 2504 - 2520
反应条件
Iron(II,III) oxide nanopowder
T=200 - 250°C; dowtherm AInert atmosphere;
参考文献
Goossen, Lukas J.; Mamone, Patrizia; Oppel, Christoph
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 1 p. 57 - 63
反应条件
1: tetrahydrofuran / -78 °C
2: Jones reagent
View Scheme
参考文献
Wrobel; Millen; Sredy; Dietrich; Gorham; Malamas; Kelly; Bauman; Harrison; Jones; Guinosso; Sestanj
Journal of Medicinal Chemistry, 1991 , vol. 34, # 8 p. 2504 - 2520
反应条件
diethyl ether
anschliessend mit wss. HCl;
参考文献
Otter; Shriner
Journal of the American Chemical Society, 1951 , vol. 73, p. 887,888
反应条件
1: 88 percent / pyridine / Ambient temperature
2: 77 percent / NaH / dimethylformamide
3: 64 percent / KOH / ethanol; H2O / Heating
View Scheme
参考文献
McEwen, William E.; Grossi, Anthony V.; MacDonald, Russell J.; Stamegna, Andrew P.
Journal of Organic Chemistry, 1980 , vol. 45, # 7 p. 1301 - 1308
反应条件
1: 77 percent / NaH / dimethylformamide
2: 64 percent / KOH / ethanol; H2O / Heating
View Scheme
参考文献
McEwen, William E.; Grossi, Anthony V.; MacDonald, Russell J.; Stamegna, Andrew P.
Journal of Organic Chemistry, 1980 , vol. 45, # 7 p. 1301 - 1308
反应条件
1: 77 percent / NaH / dimethylformamide
2: 64 percent / KOH / ethanol; H2O / Heating
View Scheme
参考文献
McEwen, William E.; Grossi, Anthony V.; MacDonald, Russell J.; Stamegna, Andrew P.
Journal of Organic Chemistry, 1980 , vol. 45, # 7 p. 1301 - 1308
参考文献
Schneider, Martin R.; Angerer, Erwin von; Schoenenberger, Helmut; Michel, Ralf Th.; Fortmeyer, H. P.
Journal of Medicinal Chemistry, 1982 , vol. 25, # 9 p. 1070 - 1077