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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-碘甲苯
合成路线
（共 1421 条）
624-31-7
4-碘甲苯
+
95-15-8
苯并噻吩
→
反应条件
63724-94-7
反应条件
copper(l) iodide; 1,10-phenanthroline; tert-BuOD; lithium tert-butylate in N,N'-dimethyl-N,N'-propyleneurea T=125°C; 1 h; Inert atmosphere;
参考文献
Do, Hien-Quang; Khan, Rana M. Kashif; Daugulis, Olafs
Journal of the American Chemical Society, 2008 , vol. 130, # 45 p. 15185 - 15192
123-39-7
N-甲基甲酰胺
+
624-31-7
4-碘甲苯
→
反应条件
2739-04-0
N,4'-二甲基甲酰苯胺
反应条件
[Cu8(H){S2P(OiPr)2}6](PF6); caesium carbonate in N,N-dimethyl-formamide T=120°C; Ullmann-Goldberg type coupling; 24 h;
参考文献
Wu, Cheng-Chieh; Lee, Bo-Han; Liao, Ping-Kuei; Fang, Ching-Shiang; Liu
Journal of the Chinese Chemical Society, 2012 , vol. 59, # 4 p. 480 - 484
590-93-2
2-丁炔酸
+
624-31-7
4-碘甲苯
→
反应条件
2749-93-1
1-甲基-4-丙-1-炔基苯
反应条件
bis-triphenylphosphine-palladium(II) chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1,4-di(diphenylphosphino)-butane in dimethyl sulfoxide T=80°C; 12 h; Inert atmosphere;
参考文献
Okuno, Yuri; Yamashita, Makoto; Nozaki, Kyoko
European Journal of Organic Chemistry, 2011 , # 20-21 p. 3951 - 3958
624-31-7
4-碘甲苯
+
100-66-3
苯甲醚
→
反应条件
53040-92-9
4-甲氧基-4-甲基-联苯
+
24423-07-2
(7CI,8CI)-m-(对甲苯)-苯甲醚
+
92495-53-9
反应条件
bathophenanthroline; sodium t-butanolate T=178°C; 6 h; Inert atmosphere;
参考文献
Yong, Guo-Ping; She, Wen-Long; Zhang, Yi-Man; Li, Ying-Zhou
Chemical Communications, 2011 , vol. 47, # 42 p. 11766 - 11768
766-85-8
3-碘苯甲醚
+
624-31-7
4-碘甲苯
→
反应条件
24423-07-2
(7CI,8CI)-m-(对甲苯)-苯甲醚
反应条件
1: 1-(iodo)-4-methylbenzene With [PdCl2(1,3-bis(diphenylphosphino)propane)]; tBuCH2CH2B(H)NiPr2; triethylamine; potassium iodide in toluene T=110°C; Suzuki coupling; 1 h; Inert atmosphere; 2: 3-methoxy-iodobenzene With caesium carbonate in ethanol; water; toluene T=90°C; Suzuki coupling; 15 h; Inert atmosphere;
参考文献
Marciasini, Ludovic; Richy, Nicolas; Vaultier, Michel; Pucheault, Mathieu
Chemical Communications, 2012 , vol. 48, # 10 p. 1553 - 1555
624-31-7
4-碘甲苯
+
100-66-3
苯甲醚
+
71-43-2
苯
→
反应条件
644-08-6
4-甲基联苯
+
53040-92-9
4-甲氧基-4-甲基-联苯
+
24423-07-2
(7CI,8CI)-m-(对甲苯)-苯甲醚
+
92495-53-9
反应条件
bathophenanthroline; sodium t-butanolate T=172°C; 12 h; Inert atmosphere;
参考文献
Shirakawa, Eiji; Itoh, Ken-Ichi; Higashino, Tomohiro; Hayashi, Tamio
Journal of the American Chemical Society, 2010 , vol. 132, # 44 p. 15537 - 15539
624-31-7
4-碘甲苯
+
100-66-3
苯甲醚
+
100-47-0
苯甲腈
+
71-43-2
苯
→
反应条件
50670-50-3
4-氰基-4'-甲基联苯
+
644-08-6
4-甲基联苯
+
53040-92-9
4-甲氧基-4-甲基-联苯
+
24423-07-2
(7CI,8CI)-m-(对甲苯)-苯甲醚
+
92495-53-9
+
114772-53-1
2-氰基-4'-甲基联苯
+
133909-96-3
4-甲基-[1,1-联苯]-3-甲腈
反应条件
bathophenanthroline; sodium t-butanolate T=178°C; 6 h; Inert atmosphere;
参考文献
Shirakawa, Eiji; Itoh, Ken-Ichi; Higashino, Tomohiro; Hayashi, Tamio
Journal of the American Chemical Society, 2010 , vol. 132, # 44 p. 15537 - 15539
624-31-7
4-碘甲苯
+
768-60-5
→
反应条件
24785-38-4
反应条件
C20H29Cl2N5O2Pd; potassium carbonate in ethanol T=80°C; Sonogashira Cross-Coupling; 2 h;
参考文献
Savicheva, Elizaveta A.; Kurandina, Daria V.; Nikiforov, Vladimir A.; Boyarskiy, Vadim P.
Tetrahedron Letters, 2014 , vol. 55, # 13 p. 2101 - 2103
624-31-7
4-碘甲苯
+
696-62-8
+
1066-54-2
→
反应条件
24785-38-4
反应条件
1: para-iodoanisole; trimethylsilylacetylene With potassium carbonate in methanol; acetonitrile T=40°C; Sonogashira Cross-Coupling; 2 h; 2: 1-(iodo)-4-methylbenzene in methanol; acetonitrile T=40°C; Sonogashira Cross-Coupling; 2 h; chemoselective reaction;
参考文献
Mandali, Pavan Kumar; Chand, Dillip Kumar
Catalysis Communications, 2014 , vol. 47, p. 40 - 44
624-31-7
4-碘甲苯
+
3989-14-8
→
反应条件
24785-38-4
反应条件
KOC(O)Ph; triphenylphosphine; copper(l) chloride in 1,3-dimethyl-imidazolidin-2-one T=120°C; Sila-Sonogashira-Hagihara cross-coupling reaction; 12 h; Inert atmosphere;
参考文献
Ihara, Hideki; Ueda, Akinori; Suginome, Michinori
Chemistry Letters, 2011 , vol. 40, # 9 p. 972 - 974
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