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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-碘甲苯
合成路线
（共 1421 条）
624-31-7
4-碘甲苯
+
363-72-4
五氟苯
→
反应条件
14621-04-6
反应条件
P(t-Bu)2Me*HBF4; silver trifluoromethanesulfonate; potassium carbonate; palladium diacetate in N,N-dimethyl acetamide T=120°C;
参考文献
Lafrance, Marc; Rowley, Christopher N.; Woo, Tom K.; Fagnou, Keith
Journal of the American Chemical Society, 2006 , vol. 128, # 27 p. 8754 - 8756
624-31-7
4-碘甲苯
+
58521-27-0
→
反应条件
14621-04-6
反应条件
copper(l) iodide in diethylene glycol dimethyl ether T=130°C; 24 h; Inert atmosphere;
参考文献
Shang, Rui; Fu, Yao; Wang, Yan; Xu, Qing; Yu, Hai-Zhu; Liu, Lei
Angewandte Chemie - International Edition, 2009 , vol. 48, # 49 p. 9350 - 9354
624-31-7
4-碘甲苯
+
327-54-8
1,2,4,5-四氟苯
+
363-72-4
五氟苯
→
反应条件
906366-85-6
+
14621-04-6
反应条件
potassium phosphate; 1,10-phenanthroline; copper(l) iodide in N,N-dimethyl-formamide T=125°C; 15 h;
参考文献
THE UNIVERSITY OF HOUSTON SYSTEM
Patent: US2009/76266 A1, 2009 ;
Location in patent: Page/Page column 28 ;
624-31-7
4-碘甲苯
→
反应条件
14621-04-6
反应条件
potassium carbonate; triphenylphosphine; silver(l) oxide; palladium diacetate in toluene T=100°C; 3 h;
参考文献
Frohn; Adonin; Bardin; Starichenko
Tetrahedron Letters, 2002 , vol. 43, # 45 p. 8111 - 8114
624-31-7
4-碘甲苯
+
1582-24-7
五氟苯硼酸
→
反应条件
14621-04-6
反应条件
1: pentafluorophenyldihydroxyborane With KHF2 in methanol; water T=20°C; 4 h; 2: 1-(iodo)-4-methylbenzene With silver(l) oxide; bis-triphenylphosphine-palladium(II) chloride in toluene T=100°C; Suzuki-Miyaura cross-coupling; 8 h; Further stages.;
参考文献
Adonin, Nicolay Yu.; Babushkin, Dmitrii E.; Parmon, Valentin N.; Bardin, Vadim V.; Kostin, Gennadiy A.; Mashukov, Vasiliy I.; Frohn, Hermann-Josef
Tetrahedron, 2008 , vol. 64, # 25 p. 5920 - 5924
344-04-7
溴五氟苯
+
624-31-7
4-碘甲苯
→
反应条件
14621-04-6
反应条件
1-butyl-2,2'-bipyridinium bis(trifluoromethanesulfonyl)amide; copper T=75°C; 20 h;
参考文献
Xiao, Ji-Chang; Ye, Chengfeng; Shreeve, Jean'ne M.
Organic Letters, 2005 , vol. 7, # 10 p. 1963 - 1965
624-31-7
4-碘甲苯
+
363-72-4
五氟苯
+
455-13-0
4-碘三氟甲苯
→
反应条件
14621-04-6
反应条件
potassium phosphate; 1,10-phenanthroline; copper(l) iodide in N,N-dimethyl-formamide T=125°C; 1 h; Product distribution / selectivity;
参考文献
THE UNIVERSITY OF HOUSTON SYSTEM
Patent: US2009/76266 A1, 2009 ;
Location in patent: Page/Page column 28 ;
624-31-7
4-碘甲苯
+
1015-53-8
→
反应条件
14621-04-6
反应条件
(i) (heating), (ii) Mg, H2SO4; Multistep reaction;
参考文献
Coe,P.L.; Pearl,G.M.
Journal of Organometallic Chemistry, 1971 , vol. 31, p. 55 - 57
127591-24-6
+
624-31-7
4-碘甲苯
→
反应条件
21209-78-9
反应条件
PdCl2(dppf) (1 molpercent) in acetonitrile byproducts: C6H4(CH3)(C6H4)OCH3; 24 h;
参考文献
Hashmi, A. Stephen K.; Lothschuetz, Christian; Doepp, Rene; Rudolph, Matthias; Ramamurthi, Tanuja D.; Rominger, Frank
Angewandte Chemie - International Edition, 2009 , vol. 48, # 44 p. 8243 - 8246
1004759-93-6
+
624-31-7
4-碘甲苯
→
反应条件
21209-78-9
反应条件
PdCl2(dppf) (1 molpercent) in acetonitrile byproducts: CH3C6H4C16H9; 24 h;
参考文献
Hashmi, A. Stephen K.; Lothschuetz, Christian; Doepp, Rene; Rudolph, Matthias; Ramamurthi, Tanuja D.; Rominger, Frank
Angewandte Chemie - International Edition, 2009 , vol. 48, # 44 p. 8243 - 8246
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