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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-碘甲苯
合成路线
（共 1421 条）
109-04-6
邻溴吡啶
+
624-31-7
4-碘甲苯
+
471-25-0
丙炔酸
→
反应条件
2789-88-0
1,1'-(1,2-乙炔二基)二(4-甲基苯)
+
80221-14-3
反应条件
bis-triphenylphosphine-palladium(II) chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1,4-di(diphenylphosphino)-butane in dimethyl sulfoxide T=50 - 80°C;
参考文献
Park, Kyungho; Bae, Goun; Moon, Jeongju; Choe, Jaehoon; Song, Kwang Ho; Lee, Sunwoo
Journal of Organic Chemistry, 2010 , vol. 75, # 18 p. 6244 - 6251
109-04-6
邻溴吡啶
+
624-31-7
4-碘甲苯
+
1066-54-2
三甲基乙炔基硅
→
反应条件
80221-14-3
反应条件
1: 2-bromo-pyridine; trimethylsilylacetylene With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine; triphenylphosphine in toluene T=25 - 80°C; Sonogashira coupling; 16.0833 h; Inert atmosphere; 2: With water; potassium hydroxide in methanol; toluene T=25°C; 3 h; Inert atmosphere; 3: 1-(iodo)-4-methylbenzene in methanol; water; toluene T=25°C; Sonogashira coupling; 16 h; Inert atmosphere;
参考文献
Severin, Rene; Reimer, Jessica; Doye, Sven
Journal of Organic Chemistry, 2010 , vol. 75, # 10 p. 3518 - 3521
870-46-2
肼基甲酸叔丁酯
+
624-31-7
4-碘甲苯
→
反应条件
820209-69-6
反应条件
air; 1,8-diazabicyclo[5.4.0]undec-7-ene; palladium diacetate in tetrahydrofuran T=110°C; 0.116667 h; microwave irradiation;
参考文献
Herrero, Maria Antonia; Wannberg, Johan; Larhed, Mats
Synlett, 2004 , # 13 p. 2335 - 2338
1514-82-5
2-溴-3,3,3-三氟丙烯
+
624-31-7
4-碘甲苯
→
反应条件
82203-82-5
反应条件
1: 2-Bromo-3,3,3-trifluoro-propene With ZnCl2*TMEDA; lithium diisopropyl amide in tetrahydrofuran; hexane T=-78 - 20°C; 1 h; 2: 1-(iodo)-4-methylbenzene With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; hexane 6 h; Heating;
参考文献
Konno, Tsutomu; Chae, Jungha; Kanda, Masashi; Nagai, Go; Tamura, Kazushige; Ishihara, Takashi; Yamanaka, Hiroki
Tetrahedron, 2003 , vol. 59, # 38 p. 7571 - 7580
624-31-7
4-碘甲苯
→
反应条件
824431-53-0
反应条件
1: PPh3; NaOH / palladium(II) acetate / tetrahydrofuran / Heating 2: 2.06 g / hydrochloric acid / tetrahydrofuran / 4 h / 20 °C 3: 82 percent / I2; PPh3; imidazole / CH2Cl2 / 0 - 20 °C View Scheme
参考文献
Belanger, Guillaume; Levesque, Francois; Paquet, Julie; Barbe, Guillaume
Journal of Organic Chemistry, 2005 , vol. 70, # 1 p. 291 - 296
97-99-4
+
624-31-7
4-碘甲苯
→
反应条件
828254-77-9
反应条件
caesium carbonate; [Cu8(S2P(OiPr)2)6(μ8-Cl)][PF6] T=110°C; 4 h;
参考文献
Manbeck, Gerald F.; Lipman, Adam J.; Stockland Jr., Robert A.; Freidl, Adrienne L.; Hasler, Amy F.; Stone, Joshua J.; Guzei, Ilia A.
Journal of Organic Chemistry, 2005 , vol. 70, # 1 p. 244 - 250
624-31-7
4-碘甲苯
→
反应条件
832744-33-9
反应条件
1: NBS; benzoyl peroxide / CCl4 / 12 h / Heating 2: dimethylformamide / 12 h / 80 °C View Scheme
参考文献
Orita, Akihiro; Miyamoto, Kazuhiko; Nakashima, Mikio; Ye, Fangguo; Otera, Junzo
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 7 p. 767 - 776
624-31-7
4-碘甲苯
→
反应条件
834-15-1
反应条件
tellurium; potassium hydroxide in dimethyl sulfoxide T=110°C; 10 h; Inert atmosphereSealed tube; Reagent/catalystSolvent;
参考文献
Zhang, Shaozhong; Karra, Kranthi; Koe, Adam; Jin, Jin
Tetrahedron Letters, 2013 , vol. 54, # 20 p. 2452 - 2454
624-31-7
4-碘甲苯
+
100-51-6
→
反应条件
834-25-3
反应条件
1,10-phenanthroline; copper(II) ferrite; caesium carbonate T=110°C; 12 h; Inert atmosphere;
参考文献
Yang, Shuliang; Xie, Wenbing; Zhou, Hua; Wu, Cunqi; Yang, Yanqin; Niu, Jiajia; Yang, Wei; Xu, Jingwei
Tetrahedron, 2013 , vol. 69, # 16 p. 3415 - 3418
624-31-7
4-碘甲苯
→
反应条件
834-25-3
反应条件
1.1: copper(l) iodide; 8-Hydroxyquinoline 1-oxide / dimethyl sulfoxide / 0.17 h / 20 °C / Inert atmosphere 1.2: 18 h / 100 °C / Inert atmosphere 2.1: cesium hydroxide monohydrate; tetra-(n-butyl)ammonium iodide / water; dimethyl sulfoxide / 12 h / 100 °C / Inert atmosphere View Scheme
参考文献
Yang, Kai; Li, Zheng; Wang, Zhaoyang; Yao, Zhiyi; Jiang, Sheng
Organic Letters, 2011 , vol. 13, # 16 p. 4340 - 4343
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