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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-碘甲苯
合成路线
（共 1421 条）
624-31-7
4-碘甲苯
+
100-66-3
苯甲醚
+
71-43-2
苯
→
反应条件
644-08-6
4-甲基联苯
+
53040-92-9
4-甲氧基-4-甲基-联苯
+
24423-07-2
(7CI,8CI)-m-(对甲苯)-苯甲醚
+
92495-53-9
反应条件
bathophenanthroline; sodium t-butanolate T=172°C; 12 h; Inert atmosphere;
参考文献
Shirakawa, Eiji; Itoh, Ken-Ichi; Higashino, Tomohiro; Hayashi, Tamio
Journal of the American Chemical Society, 2010 , vol. 132, # 44 p. 15537 - 15539
624-31-7
4-碘甲苯
+
100-66-3
苯甲醚
+
100-47-0
苯甲腈
+
71-43-2
苯
→
反应条件
50670-50-3
4-氰基-4'-甲基联苯
+
644-08-6
4-甲基联苯
+
53040-92-9
4-甲氧基-4-甲基-联苯
+
24423-07-2
(7CI,8CI)-m-(对甲苯)-苯甲醚
+
92495-53-9
+
114772-53-1
2-氰基-4'-甲基联苯
+
133909-96-3
4-甲基-[1,1-联苯]-3-甲腈
反应条件
bathophenanthroline; sodium t-butanolate T=178°C; 6 h; Inert atmosphere;
参考文献
Shirakawa, Eiji; Itoh, Ken-Ichi; Higashino, Tomohiro; Hayashi, Tamio
Journal of the American Chemical Society, 2010 , vol. 132, # 44 p. 15537 - 15539
624-31-7
4-碘甲苯
+
661-69-8
六甲基二锡
→
反应条件
937-12-2
反应条件
[PdBr2(PPh3)2] in toluene byproducts: Me3SnI; at 115°C for 15 h in sealed thick wall Pyrex glass ampoules;
参考文献
Azizian, Hormoz; Eaborn, Colin; Pidcock, Alan
Journal of Organometallic Chemistry, 1981 , vol. 215, # 1 p. 49 - 58
4333-56-6
溴代环丙烷
+
624-31-7
4-碘甲苯
→
反应条件
6921-43-3
1-环丙基-4-甲基苯
反应条件
1: cyclopropyl bromide With tert.-butyl lithium in diethyl ether; pentane T=-78 - 20°C; 2: With indium(III) chloride in tetrahydrofuran; diethyl ether; pentane T=-78 - 20°C; 3: 1-(iodo)-4-methylbenzene With bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran; diethyl ether; pentane 3 h; Heating; Further stages.;
参考文献
Perez, Ignacio; Sestelo, Jose Perez; Sarandeses, Luis A.
Organic Letters, 1999 , vol. 1, # 8 p. 1267 - 1269
624-31-7
4-碘甲苯
+
23719-81-5
→
反应条件
6921-43-3
1-环丙基-4-甲基苯
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran 3 h; Heating;
参考文献
Perez; Sestelo; Sarandeses
Journal of the American Chemical Society, 2001 , vol. 123, # 18 p. 4155 - 4160
624-31-7
4-碘甲苯
+
103-67-3
N-甲基苄胺
→
反应条件
69267-39-6
反应条件
tris-(dibenzylideneacetone)dipalladium(0); tris-(o-tolyl)phosphine; sodium t-butanolate in 1,4-dioxane T=100°C; 4.5 h;
参考文献
Wolfe, John P.; Buchwald, Stephen L.
Journal of Organic Chemistry, 1996 , vol. 61, # 3 p. 1133 - 1135
624-31-7
4-碘甲苯
→
反应条件
93627-32-8
反应条件
1: 15 g / copper powder / 4 h / 190 - 200 °C 2: 0.9 g / conc. H2SO4 chromium trioxide / acetic acid / 4 h / Ambient temperature 3: 0.25 g / anhyd. triethyl phosphite / 8 h / 170 °C 4: 0.33 g / HCl(10percent) / methanol / 0.5 h / Heating 5: 85 percent / aq. NaOH (5percent) / 4 h / Ambient temperature 6: 60 percent / H2 / Pd/C (10percent) / methanol / 0.5 h / Ambient temperature View Scheme
参考文献
Bhatia, S. K.; Kapil, R. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 4 p. 296 - 299
624-31-7
4-碘甲苯
+
112-55-0
十二硫醇
→
反应条件
94435-76-4
反应条件
copper(I) oxide; potassium hydroxide in 1,4-dioxane T=110°C; 6 h; Inert atmosphere;
参考文献
Kao, Hsin-Lun; Chen, Chin-Keng; Wang, Yu-Jen; Lee, Chin-Fa
European Journal of Organic Chemistry, 2011 , # 9 p. 1776 - 1781
624-31-7
4-碘甲苯
+
112-55-0
十二硫醇
→
反应条件
反应条件
copper(I) oxide; potassium tert-butylate in N,N-dimethyl-formamide T=110°C; 6 h; Inert atmosphere;
参考文献
Kao, Hsin-Lun; Chen, Chin-Keng; Wang, Yu-Jen; Lee, Chin-Fa
European Journal of Organic Chemistry, 2011 , # 9 p. 1776 - 1781
292638-84-7
+
624-31-7
4-碘甲苯
→
反应条件
4714-21-0
+
948-55-0
反应条件
C18H19Cl2N2PPd; triethylamine in N,N-dimethyl-formamide T=140°C; Heck Reaction; 21 h; Inert atmosphereSchlenk technique;
参考文献
Suarez-Meneses, Jesus V.; Bonilla-Reyes, Edgar; Ble-Gonzalez, Ever A.; Ortega-Alfaro, M. Carmen; Toscano, Ruben Alfredo; Cordero-Vargas, Alejandro; Lopez-Cortes, Jose G.
Tetrahedron, 2014 , vol. 70, # 7 p. 1422 - 1430
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