1: isopropylmagnesium chloride With indium(III) chloride in tetrahydrofuran; hexane
T=-78 - 20°C;
2: carbon monoxide; 1-(iodo)-4-methylbenzene With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; hexane
T=60°C; 1 h;
参考文献
Lee, Sung Wook; Lee, Kooyeon; Seomoon, Dong; Kim, Sundae; Kim, Hyunseok; Kim, Hyun; Shim, Eunkyong; Lee, Miae; Lee, Seokju; Kim, Misook; Lee, Phil Ho
Journal of Organic Chemistry, 2004 , vol. 69, # 14 p. 4852 - 4855
copper(I) oxide in acetonitrile
10 h; Reflux; Reagent/catalyst;
参考文献
Costa, Marcio V.; Viana, Gil M.; De Souza, Thais M.; Malta, Luiz Fernando B.; Aguiar, Lucia C.S.
Tetrahedron Letters, 2013 , vol. 54, # 19 p. 2332 - 2335