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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-碘甲苯
合成路线
（共 1421 条）
124-22-1
十二烷基伯胺
+
624-31-7
4-碘甲苯
→
反应条件
62641-34-3
反应条件
anhydrous iron chloride; caesium carbonate; copper(II) oxide; 1,1'-binaphthyl-2,2'-diol in N,N-dimethyl-formamide T=90°C; 12 h; Inert atmosphere;
参考文献
Wang, Zhe; Fu, Hua; Jiang, Yuyang; Zhao, Yufen
Synlett, 2008 , # 16 p. 2540 - 2546
288-42-6
恶唑
+
624-31-7
4-碘甲苯
→
反应条件
62882-04-6
2-(4-甲基苯基)恶唑
反应条件
1: 1,3-oxazole With n-butyllithium; zinc(II) chloride in tetrahydrofuran; hexane T=-78 - 20°C; Negishi coupling reaction; 2: 1-(iodo)-4-methylbenzene With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=60°C; 4 h; Further stages.;
参考文献
Ohnmacht, Stephan A.; Mamone, Patrizia; Culshaw, Andrew J.; Greaney, Michael F.
Chemical Communications, 2008 , # 10 p. 1241 - 1243
624-31-7
4-碘甲苯
→
反应条件
6293-68-1
4,4'-二甲基二苯基碘鎓
反应条件
(NH4)2S2O8 in sulfuric acid; toluene
参考文献
Nippon Petrochemicals Co., Ltd.
Patent: US4659840 A1, 1987 ;
624-31-7
4-碘甲苯
+
108-24-7
乙酸酐
+
108-88-3
甲苯
→
反应条件
90347-65-2
+
6293-70-5
反应条件
1: With sulfuric acid in acetic acid Electrolysis; 2: With potassium iodide in water
参考文献
Peacock; Pletcher
Tetrahedron Letters, 2000 , vol. 41, # 46 p. 8995 - 8998
624-31-7
4-碘甲苯
+
108-88-3
甲苯
→
反应条件
6293-70-5
反应条件
1: sulfuric acid; acetic anhydride / water; acetonitrile / 0 h / 25 °C / Electrolysis 2: potassium iodide / water View Scheme
参考文献
Watts, Kevin; Gattrell, William; Wirth, Thomas
Beilstein Journal of Organic Chemistry, 2011 , vol. 7, p. 1108 - 1114
98-10-2
苯磺酰胺
+
624-31-7
4-碘甲苯
→
反应条件
6311-65-5
反应条件
copper(l) iodide; potassium carbonate; N-methyl-2-(methylamino)ethylamine in acetonitrile T=40°C; 8 h; Inert atmosphere;
参考文献
Wang, Xiang; Guram, Anil; Ronk, Michael; Milne, Jacqueline E.; Tedrow, Jason S.; Faul, Margaret M.
Tetrahedron Letters, 2012 , vol. 53, # 1 p. 7 - 10
938-10-3
苯磺酰基叠氮化物
+
624-31-7
4-碘甲苯
→
反应条件
6311-65-5
反应条件
copper(l) iodide; 1,10-phenanthroline; Cu; potassium carbonate in N,N-dimethyl-formamide T=110°C; 24 h;
参考文献
Yavari; Solgi; Ghazanfarpour-Darjani; Ahmadian
Journal of the Iranian Chemical Society, 2012 , vol. 9, # 6 p. 977 - 981
109-04-6
邻溴吡啶
+
624-31-7
4-碘甲苯
→
反应条件
51263-27-5
反应条件
1: 1-(iodo)-4-methylbenzene With potassium phosphate; copper(l) iodide; lithium amide in N,N-dimethyl-formamide T=130°C; 6 h; Inert atmosphere; 2: 2-bromo-pyridine in N,N-dimethyl-formamide T=130°C; 18 h; Inert atmosphere; chemoselective reaction;
参考文献
Tlili, Anis; Monnier, Florian; Taillefer, Marc
Chemical Communications, 2012 , vol. 48, # 51 p. 6408 - 6410
930-68-7
2-环己烯-1-酮
+
624-31-7
4-碘甲苯
→
反应条件
6330-12-7
反应条件
sodium acetate; 1H-tetrazole; palladium in N,N-dimethyl-formamide T=120°C; Heck reaction; 12 h;
参考文献
Gupta, Arun Kumar; Song, Chung Hyun; Oh, Chang Ho
Tetrahedron Letters, 2004 , vol. 45, # 21 p. 4113 - 4116
269410-07-3
+
624-31-7
4-碘甲苯
→
反应条件
64586-14-7
反应条件
Pd0(tris(tert-butyl)phosphine)2; water; caesium carbonate in ethylene glycol dimethyl ether T=80°C; Suzuki-Miyaura cross-coupling reaction; 52 h; Inert atmosphere;
参考文献
Yoshida, Hiroto; Okada, Kengo; Kawashima, Shota; Tanino, Kenji; Ohshita, Joji
Chemical Communications, 2010 , vol. 46, # 10 p. 1763 - 1765
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