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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-碘甲苯
合成路线
（共 1421 条）
624-31-7
4-碘甲苯
→
反应条件
4714-21-0
4-甲基二苯乙烯
反应条件
tetrabutyl ammonium fluoride; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in tetrahydrofuran T=60°C; 1 h;
参考文献
Mori; Suguro
Synlett, 2001 , # 6 p. 845 - 847
624-31-7
4-碘甲苯
+
6783-05-7
反式-BETA-苯乙烯硼酸
→
反应条件
4714-21-0
4-甲基二苯乙烯
反应条件
caesium carbonate; [Pt(PPh3)4] in N,N-dimethyl-formamide T=120°C; Suzuki reaction; 12 h;
参考文献
Oh, Chang Ho; Lim, Young Mook; You, Choong Ho
Tetrahedron Letters, 2002 , vol. 43, # 26 p. 4645 - 4648
624-31-7
4-碘甲苯
+
72761-85-4
→
反应条件
4714-21-0
4-甲基二苯乙烯
反应条件
tris-(o-tolyl)phosphine; potassium hydroxide; bis(dibenzylideneacetone)-palladium(0) in methanol T=70°C; 16 h; optical yield given as percent de;
参考文献
Sore, Hannah F.; Boehner, Christine M.; Laraia, Luca; Logoteta, Patrizia; Prestinari, Cora; Scott, Matthew; Williams, Katharine; Galloway, Warren R. J. D.; Spring, David R.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 2 p. 504 - 515
624-31-7
4-碘甲苯
+
1566-65-0
→
反应条件
4714-21-0
4-甲基二苯乙烯
反应条件
tributyl-amine; montmorilloniteethylsilyldiphenylphosphine palladium(II) chloride T=100°C; 6 h;
参考文献
Choudary, Boyapati M.; Sarma, Ravichandra M.; Rao, Koteswara K.
Tetrahedron, 1992 , vol. 48, # 4 p. 719 - 726
624-31-7
4-碘甲苯
+
1177254-28-2
→
反应条件
4714-21-0
4-甲基二苯乙烯
反应条件
bis(η3-allyl-μ-chloropalladium(II)); tetrabutyl ammonium fluoride in tetrahydrofuran T=65°C; Hiyama coupling; 1 h; Inert atmosphere; stereoselective reaction;
参考文献
Pawluc, Piotr; Hreczycho, Grzegorz; Suchecki, Andrzej; Kubicki, Maciej; Marciniec, Bogdan
Tetrahedron, 2009 , vol. 65, # 28 p. 5497 - 5502
624-31-7
4-碘甲苯
+
66680-87-3
→
反应条件
4714-21-0
4-甲基二苯乙烯
反应条件
diphenylphosphine-based palladium(0) complex on MCM-41 in water; N,N-dimethyl-formamide T=60°C; Stille coupling; 8 h;
参考文献
Zhao, Hong; Wang, Yue; Sha, Junchao; Sheng, Shouri; Cai, Mingzhong
Tetrahedron, 2008 , vol. 64, # 32 p. 7517 - 7523
624-31-7
4-碘甲苯
+
140-10-3
肉桂酸
→
反应条件
4714-21-0
4-甲基二苯乙烯
反应条件
silver carbonate; palladium dichloride; 2-dicyclohexylphosphino-1,1'-biphenyl in N,N-dimethyl acetamide T=150°C; 12 h; Inert atmosphere;
参考文献
Wang, Zhiyong; Ding, Qiuping; He, Xiaodan; Wu, Jie
Organic and Biomolecular Chemistry, 2009 , vol. 7, # 5 p. 863 - 865
624-31-7
4-碘甲苯
+
72761-85-4
→
反应条件
4714-21-0
4-甲基二苯乙烯
+
948-55-0
反应条件
potassium hydroxide; bis(dibenzylideneacetone)-palladium(0) in methanol T=20°C; Inert atmosphere;
参考文献
Sore, Hannah F.; Boehner, Christine M.; Laraia, Luca; Logoteta, Patrizia; Prestinari, Cora; Scott, Matthew; Williams, Katharine; Galloway, Warren R. J. D.; Spring, David R.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 2 p. 504 - 515
624-31-7
4-碘甲苯
+
439659-78-6
→
反应条件
4714-21-0
4-甲基二苯乙烯
反应条件
bis(η3-allyl-μ-chloropalladium(II)) in tetrahydrofuran T=20°C; 1 h;
参考文献
Katayama, Hiroyuki; Taniguchi, Ken; Kobayashi, Masayuki; Sagawa, Takashi; Minami, Tatsuya; Ozawa, Fumiyuki
Journal of Organometalic Chemistry, 2002 , vol. 645, # 1-2 p. 192 - 200
624-31-7
4-碘甲苯
+
155857-33-3
→
反应条件
4714-21-0
4-甲基二苯乙烯
+
948-55-0
反应条件
bis(η3-allyl-μ-chloropalladium(II)); tetrabutyl ammonium fluoride in tetrahydrofuran T=60°C; 14 h; Yield given. Yields of byproduct given;
参考文献
Hatanaka, Yasuo; Goda, Ken-ichi; Hiyama, Tamejiro
Journal of Organometallic Chemistry, 1994 , vol. 465, # 1-2 p. 97 - 100
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