反应条件
1: phenyllithium With DABCO-bis(sulfur dioxide) in 1,4-dioxane T=-40 - 20°C; 2 h; Inert atmosphereSchlenk technique; 2: 1-(iodo)-4-methylbenzene With palladium diacetate; caesium carbonate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene T=85°C; 16 h; Inert atmosphereSchlenk technique; SolventReagent/catalystTemperature;
参考文献
Emmett, Edward J.; Hayter, Barry R.; Willis, Michael C.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 48 p. 12679 - 12683
Angew. Chem., 2013 , vol. 125, # 48 p. 12911 - 12915,5
