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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-碘甲苯
合成路线
（共 1421 条）
201230-82-2
+
624-31-7
4-碘甲苯
+
100-44-7
苄基氯
→
反应条件
2001-28-7
4-甲基-2-苯基苯乙酮
反应条件
palladium diacetate; 1,4-di(diphenylphosphino)-butane; zinc in 1,4-dioxane T=100°C; Negishi coupling reaction; P=7500.75 Torr; 16 h; Inert atmosphereAutoclave;
参考文献
Chemistry - An Asian Journal, , vol. 7, # 1 p. 40 - 44
60-35-5
乙酰胺
+
624-31-7
4-碘甲苯
→
反应条件
103-89-9
4'-甲基乙酰苯胺
反应条件
potassium phosphate; copper(l) iodide; glycine in 1,4-dioxane T=100°C; Goldberg reaction; 24 h;
参考文献
Deng, Wei; Wang, Ye-Feng; Zou, Yan; Liu, Lei; Guo, Qing-Xiang
Tetrahedron Letters, 2004 , vol. 45, # 11 p. 2311 - 2315
624-31-7
4-碘甲苯
+
75-05-8
乙腈
→
反应条件
103-89-9
4'-甲基乙酰苯胺
反应条件
copper(l) iodide; water; caesium carbonate; potassium hydroxide; N-methyl-2-(methylamino)ethylamine T=100°C; 15 h; Inert atmosphereSchlenk technique;
参考文献
Xiang, Shi-Kai; Zhang, Dong-Xue; Hu, Hao; Shi, Jiang-Ling; Liao, Li-Guo; Feng, Chun; Wang, Bi-Qin; Zhao, Ke-Qing; Hu, Ping; Yang, Hua; Yu, Wen-Hao
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 8 p. 1495 - 1499
624-31-7
4-碘甲苯
+
292638-85-8
丙烯酸甲酯
→
反应条件
20754-20-5
对甲基肉桂酸甲酯
反应条件
triethylamine; PdCl2(4,4'-bis(n-C10F21CH2OCH2)-2,2'-bpy) in N,N-dimethyl-formamide T=140°C; Heck reaction; 5 h;
参考文献
Lu, Norman; Chen, Shih-Chieh; Chen, Tsung-Chi; Liu, Ling-Kang
Tetrahedron Letters, 2008 , vol. 49, # 2 p. 371 - 375
624-31-7
4-碘甲苯
+
292638-85-8
丙烯酸甲酯
→
反应条件
50363-84-3
+
20754-20-5
对甲基肉桂酸甲酯
反应条件
potassium acetate; β-ketoesterato polymeric palladium in N,N-dimethyl-formamide T=90°C; Heck coupling reaction; 4 h;
参考文献
European Journal of Inorganic Chemistry, , # 5 p. 1094 - 1099
624-31-7
4-碘甲苯
+
292638-85-8
丙烯酸甲酯
→
反应条件
20754-20-5
对甲基肉桂酸甲酯
+
108-88-3
反应条件
sodium carbonate; triphenylphosphine; Pt(COD)Cl2 in various solvent(s) T=130°C; 24 h; Yield given. Yields of byproduct given;
参考文献
Kelkar, Ashutosh A.
Tetrahedron Letters, 1996 , vol. 37, # 49 p. 8917 - 8920
624-31-7
4-碘甲苯
+
696-62-8
+
292638-85-8
丙烯酸甲酯
→
反应条件
20754-20-5
对甲基肉桂酸甲酯
+
3901-07-3
反应条件
tributyl-amine; montmorilloniteethylsilyldiphenylphos.. T=100°C; competition reaction; relative rates of S1/S2 in individual reaction; substrate selectivity; Kinetics;
参考文献
Choudary, B. M.; Sarma, M. Ravichandra; Rao, K. Koteswara
Tetrahedron Letters, 1990 , vol. 31, # 40 p. 5781 - 5784
624-31-7
4-碘甲苯
+
73183-34-3
→
反应条件
195062-57-8
反应条件
copper(l) iodide; tributylphosphine; potassium tert-butylate in tetrahydrofuran react. of 4-MeC6H4I (1 equv.), B2pin2 (1.5 equiv.), nBu3P (13 molpercent), KOtBu (1.5 equiv.) and CuI (10 molpercent) at room temp. for 24 h;
参考文献
Kleeberg, Christian; Dang, Li; Lin, Zhenyang; Marder, Todd B.
Angewandte Chemie, International Edition, 2009 , vol. 48, p. 5350 - 5354
Angewandte Chemie, 2009 , vol. 121, p. 5454 - 5458
76-09-5
+
624-31-7
4-碘甲苯
→
反应条件
195062-57-8
反应条件
1: 1-(iodo)-4-methylbenzene With tBuCH2CH2B(H)NiPr2; triethylamine; triphenylphosphine; palladium dichloride in tetrahydrofuran T=65°C; Alcaraz-Vaultier borylation; 12 h; Inert atmosphere; 2: 2,3-dimethylbutane-2,3-diol in tetrahydrofuran T=0 - 25°C; 0.25 h; Inert atmosphere; Further stages;
参考文献
Haddenham, Dustin; Bailey, Christopher L.; Vu, Chau; Nepomuceno, Gabby; Eagon, Scott; Pasumansky, Lubov; Singaram, Bakthan
Tetrahedron, 2011 , vol. 67, # 3 p. 576 - 583
624-31-7
4-碘甲苯
+
25015-63-8
→
反应条件
195062-57-8
反应条件
triethylamine; σ4,λ5-phosphinine palladium in 1,4-dioxane; toluene T=80°C; Myaura cross-coupling reaction; 48 h;
参考文献
Doux, Marjolaine; Mezailles, Nicolas; Melaimi, Mohand; Ricard, Louis; Le Floch, Pascal
Chemical Communications, 2002 , # 15 p. 1566 - 1567
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