1: 11 percent / Cu / 1 h / 210 °C 2: 42.55 g / diisobutylaluminum hydride / toluene / 0.25 h / -78 - -70 °C 3: pyridinium chlorochromate / CH2Cl2 / 0.5 h / 25 °C View Scheme
参考文献
Carini, David J.; Duncia, John V.; Aldrich, Paul E.; Chiu, Andrew T.; Johnson, Alexander L.; et al.
Journal of Medicinal Chemistry, 1991 , vol. 34, # 8 p. 2525 - 2547
1: thien-2-yl bromide With manganese in tetrahydrofuran T=20°C; 2 h; 2: 1-(iodo)-4-methylbenzene With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=20°C; 2 h;
