反应条件
triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane under N2 atm. to soln. 1,4-diiodobenzene in dioxane , (PdCl2(dppf)), Et3N, and (pinacolato)boron were added and mixt. was heated to 80°Cfor 12 h; H2O and CH2Cl2 were added, mixt. was filtered, org. phase was separated, dried over Na2SO4 and solvent was evapd. in vacuo, product was recrystd. from hexane; elem. anal.;
参考文献
Baehr, Anja; Felber, Beatrice; Schneider, Katharina; Diederich, Francois
Helvetica Chimica Acta, 2000 , vol. 83, # 7 p. 1346 - 1376